1-Bromo-4-decyloxybenzene

Base Information

• Chemical Name: 1-Bromo-4-decyloxybenzene
• CAS No.: 30752-20-6
• Molecular Formula: C16H25BrO
• Molecular Weight: 313.278
• DSSTox Substance ID: DTXSID70441885
• Wikidata: Q82258880
• Mol file: 30752-20-6.mol

Synonyms:1-Bromo-4-decyloxybenzene;4-n-decyloxyphenyl bromide;30752-20-6;SCHEMBL6740617;DTXSID70441885;KBAGYDCKVAKSFS-UHFFFAOYSA-N;AKOS006244311

Chemical Property of 1-Bromo-4-decyloxybenzene

Chemical Property:

• PSA: 9.23000
• LogP: 5.96860
• XLogP3: 7.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 10
• Exact Mass: 312.10888
• Heavy Atom Count: 18
• Complexity: 176

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCOC1=CC=C(C=C1)Br

Technology Process of 1-Bromo-4-decyloxybenzene

There total 7 articles about 1-Bromo-4-decyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-bromo-phenol (106-41-2) + 1-bromo dodecane (112-29-8) → 1-bromo-4-decyloxybenzene (30752-20-6)

Guidance literature:

With potassium carbonate;

DOI:10.1080/10587250108025293

Reference yield: 84.0%

4-bromo-phenol (106-41-2) + Iododecane (2050-77-3) → 1-bromo-4-decyloxybenzene (30752-20-6)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 50 ℃;

DOI:10.1021/ja304602t

Reference yield: 75.0%

4-bromo-phenol (106-41-2) + 1-bromo-octane (111-83-1) → 1-bromo-4-decyloxybenzene (30752-20-6)

Guidance literature:

With potassium carbonate; potassium iodide;

upstream raw materials:

4-bromo-phenol

1-bromo dodecane

1-bromo-octane

1-bromo-4-octyloxybenzene

Downstream raw materials:

2,7-bis((4-(decyloxy)phenyl)ethynyl)cyclopenta[hi]-aceanthrylene

2,8-bis((4-(decyloxy)phenyl)ethynyl)dicyclopenta[de,mn]-tetracene

2-(4-(decyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

(2-(4-decyloxyphenyl)ethynyl)trimethylsilane

Refernces

• 1、 Kapf, Andreas,Eslahi, Hassan,Blanke, Meik,Saccone, Marco,Giese, Michael,Albrecht, Marcel. "Alkyloxy modified pyrene fluorophores with tunable photophysical and crystalline properties". supporting information. p. 6361 - 6371. Retrieved 2019/04/25.
• 2、 W?hrle, Tobias,Gündemir, Rafet,Frey, Wolfgang,Knecht, Friederike,K?hn, Andreas,Laschat, Sabine. "Thermotropic MIDA Boronates as a Case Study for the Role of Dipolar Interactions in Liquid Crystalline Self-Assembly". supporting information. p. 4149 - 4159. Retrieved 2017/03/31.