1,2-EPOXYCYCLODECANE

Base Information

• Chemical Name: 1,2-EPOXYCYCLODECANE
• CAS No.: 286-94-2
• Molecular Formula: C₁₀H₁₈O
• Molecular Weight: 154.252
• Mol file: 286-94-2.mol

Synonyms:Cyclodecane,1,2-epoxy-; Epoxycyclodecane

Chemical Property of 1,2-EPOXYCYCLODECANE

Chemical Property:

• Refractive Index: n20/D 1.484
• PSA: 12.53000
• Density: 0.962 g/mL at 20 °C(lit.)
• LogP: 2.88820

Purity/Quality:

98%Min ^*data from raw suppliers

Cyclodecene oxide ≥96.0% (GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 1,2-EPOXYCYCLODECANE

There total 4 articles about 1,2-EPOXYCYCLODECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(Z)-cyclodecene (935-31-9) → cyclodecene oxide (286-94-2,29587-91-5)

Guidance literature:

With 1,1,1,3',3',3'-hexafluoro-propanol; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; oxygen; 1,2,3,10a-tetrahydro-dipyrrolo[1,2-a;1',2'-d]pyrazine-5,10-dione; at 20 ℃; for 12h; Green chemistry;

DOI:10.1039/d1gc03029a

Reference yield: 40.6%

trans-cyclodecene (2198-20-1) → cyclodecene oxide (286-94-2,29587-91-5)

Guidance literature:

With dihydrogen peroxide; In acetonitrile; at 60 ℃; for 5h;

DOI:10.1002/chem.201001508

Reference yield:

→ trans-1,2-epoxycyclodecane (286-94-2,29587-91-5,29587-92-6)

Guidance literature:

With Perbenzoic acid; chloroform;

DOI:10.1002/hlca.19520350526

upstream raw materials:

(Z)-cyclodecene

trans-cyclodecene

Cyclodecene

Downstream raw materials:

1-decalinol

(E/Z)-2-Cyclodecen-1-ol

(Z)-cyclodecene

trans-cyclodecene

Refernces

• 1、 Bouzari, Narges,Bezaatpour, Abolfazl,Babaei, Behnam,Amiri, Mandana,Boukherroub, Rabah,Szunerits, Sabine. "Modification of MnFe2O4 surface by Mo (VI) pyridylimine complex as an efficient nanocatalyst for (ep)oxidation of alkenes and sulfides". . . Retrieved 2021/03/04.
• 2、 Lin, Kaifeng,Lebedev, Oleg I.,Vana Tendeloo, Gustaaf,Jacobs, Pierre A.,Pescarmona, Paolo P.. "Titanosilicate beads with hierarchical porosity: Synthesis and application as epoxidation catalysts". experimental part. p. 13509 - 13518. Retrieved 2011/03/17.