N,N-Diethyl-N-methylethanaminium iodide

Base Information

• Chemical Name: N,N-Diethyl-N-methylethanaminium iodide
• CAS No.: 994-29-6
• Molecular Formula: C7H18N+
• Molecular Weight: 243.131
• Hs Code.: 2923900090
• DSSTox Substance ID: DTXSID20883630
• Mol file: 994-29-6.mol

Synonyms:994-29-6;N,N-Diethyl-N-methylethanaminium iodide;Methyltriethylammonium iodide;Ethanaminium, N,N-diethyl-N-methyl-, iodide;triethyl(methyl)azanium;iodide;Ethanaminium, N,N-diethyl-N-methyl-, iodide (1:1);N,N-Diethyl-N-methylethanaminiumiodide;Et3N-Me;SCHEMBL237968;triethyl(methyl)ammonium iodide;C7H18N.I;DTXSID20883630;AKOS016005391

Chemical Property of N,N-Diethyl-N-methylethanaminium iodide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: -1.50330
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 243.04840
• Heavy Atom Count: 9
• Complexity: 47.1

Purity/Quality:

98%Min ^*data from raw suppliers

N,N-Diethyl-N-methylethanaminium iodide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[N+](C)(CC)CC.[I-]

Technology Process of N,N-Diethyl-N-methylethanaminium iodide

There total 8 articles about N,N-Diethyl-N-methylethanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

triethylamine (121-44-8) + methyl iodide (74-88-4) → triethylmethylammonium iodide (994-29-6)

Guidance literature:

With Hexamethyldisiloxane; at 20 ℃; for 24h; Solvent; Green chemistry;

DOI:10.1039/c3gc42036a

Reference yield: 96.0%

1-iodo-N,N,N-triethylmethaniminium iodide (104304-17-8) → triethylmethylammonium iodide (994-29-6)

Guidance literature:

With tert-Amyl alcohol; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; for 0.25h; Heating; Irradiation;

DOI:10.1021/jo9813538

Reference yield:

ethyl 2-cyano-3-(3, 4-dimethoxy-5-nitrophenyl)prop-2-enoate + triethylamine (121-44-8) → ethyl 2-cyano-3-(4-hydroxy-3-methoxy-5-nitrophenyl)prop-2-enoate + triethylmethylammonium iodide (994-29-6)

Guidance literature:

ethyl 2-cyano-3-(3, 4-dimethoxy-5-nitrophenyl)prop-2-enoate; triethylamine; In ethanol; at 70 - 75 ℃; for 12h;

With hydrogen iodide; In water;

DOI:10.1007/s12039-015-0961-4

upstream raw materials:

triethylamine

methyl iodide

N,N-diethylnmethylamine

ethyl iodide

Downstream raw materials:

methane

ethane

ethene

triethylamine

Refernces

• 1、 -. "Method of producing oxyborate Tetracyanobicyclo (by machine translation)". Paragraph 0080. . Retrieved 2016/12/26.
• 2、 Ab Rani, Mohd Azri,Borduas, Nadine,Colquhoun, Victoria,Hanley, Robert,Johnson, Henry,Larger, Solene,Lickiss, Paul D.,Llopis-Mestre, Veronica,Luu, Selina,Mogstad, Martin,Oczipka, Philipp,Sherwood, James R.,Welton, Tom,Xing, Jun-Yi. "The potential of methylsiloxanes as solvents for synthetic chemistry applications". . p. 1282 - 1296. Retrieved 2014/03/21.