Germane, tributylchloro-

Base Information Edit

Chemical Name:Germane, tributylchloro-
CAS No.:2117-36-4
Molecular Formula:C12H27 Cl Ge
Molecular Weight:279.389
Hs Code.:2931900090
European Community (EC) Number:218-323-2
DSSTox Substance ID:DTXSID9062190
Nikkaji Number:J49.206J
Wikidata:Q41669766
Mol file:2117-36-4.mol

Synonyms:Germane, tributylchloro-;2117-36-4;tributyl(chloro)germane;tri-n-butylgermanium chloride;Chlorotributylgermanium;Tributylchlorogermane;Germanium, chlorotributyl-;BRN 4125563;EINECS 218-323-2;AI3-52036;Tri-n-butylgermaniumchloride;Tri-n-butylchlorogermane;CHLOROTRIBUTYLGERMANE;SCHEMBL150917;DTXSID9062190;TRIBUTYLGERMANIUM CHLORIDE;MFCD00018075;AKOS024319101;TRI-n-BUTYLCHLOROGERMANE, tech-90;LS-71216;FT-0634046

Suppliers and Price of Germane, tributylchloro-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
CHLOROTRIBUTYLGERMANE Aldrich
50mg
$ 57.00

American Custom Chemicals Corporation
TRI-N-BUTYLCHLOROGERMANE 95.00%
5MG
$ 500.32

Total 11 raw suppliers

Chemical Property of Germane, tributylchloro- Edit

Chemical Property:

Refractive Index:n20/D 1.465(lit.)
Boiling Point:270 °C(lit.)
Flash Point:>230 °F
PSA：0.00000
Density:1.054 g/mL at 25 °C(lit.)
LogP:5.57100
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:9
Exact Mass:280.1013063
Heavy Atom Count:14
Complexity:104

Purity/Quality:

98%Min ^*data from raw suppliers

CHLOROTRIBUTYLGERMANE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 34-20/21/22
Safety Statements: 45-36/37/39-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CCCC[Ge](CCCC)(CCCC)Cl

Technology Process of Germane, tributylchloro-

There total 19 articles about Germane, tributylchloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1067-42-1
tetrabutylgermanium

: 10038-98-9
germaniumtetrachloride

: 2117-36-4
tri-n-butylchlorogermane

Guidance literature:: aluminium trichloride; other Radiation; a mixt. of GeCl4 and tetraalkylgermane in presence of AlCl3 as catalystin a Pyrex tube is irradiated with a light stream of argon for 3 min atatmospheric pressure (microwave irradiation: 300 W) (Ar); identification by (1)H-NMR, gas chromy.;
DOI:10.1021/om00018a050

Reference yield: 93.0%

: 998-39-0
tributylgermanium hydride

: 98-88-4
benzoyl chloride

: 2117-36-4
tri-n-butylchlorogermane

: 100-52-7
benzaldehyde

Guidance literature:: With sodium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N,N,N,N,N-hexamethylphosphoric triamide; (N2); addn. of Bu3GeH to acylchloride and Pd-complex in HMPA, heating (1 h, 80°C), addn. of aq. NaCl; Ge compound not isolated, org. compound sepd. by chromy.;;
DOI:10.1016/0022-328X(89)88072-6

Reference yield: 92.0%

: 1067-42-1
tetrabutylgermanium

: 10038-98-9
germaniumtetrachloride

: 4593-81-1
dibutyldichlorogermane

: 2117-36-4
tri-n-butylchlorogermane

Guidance literature:: aluminium trichloride; other Radiation; a mixt. of GeCl4 and tetraalkylgermane in presence of AlCl3 as catalystin a Pyrex tube is irradiated with a light stream of argon for 30 min at atmospheric pressure (microwave irradiation: 300 W) (Ar); identification by (1)H-NMR, gas chromy.;
DOI:10.1021/om00018a050