Multi-step reaction with 10 steps
1: 24 percent / potassium hydroxide, H2 / 10percent palladium charcoal / ethanol / 0.5 h / 760 Torr / Ambient temperature
2: 91 percent / pyridine / 44 h / Ambient temperature
3: 97 percent / basic alumina
4: 94 percent / LAH / diethyl ether / 12 h / Heating
5: 92 percent / chromium trioxide / pyridine / 3 h / Ambient temperature
6: 99 percent / boron trifluoride etherate / benzene / 4 h / Ambient temperature
7: 76 percent / etheral methyllithium / tetrahydrofuran / 0.33 h / 0 °C
8: 77 percent / ozone, sodium borohydride / methanol; CH2Cl2 / 0.58 h / -77 °C
9: 84 percent / tri-n-butyl phosphine / tetrahydrofuran; pyridine / 18 h / Ambient temperature
10: 72 percent / NaHCO3, NaIO4 / methanol; tetrahydrofuran; H2O / 6 h / Ambient temperature
With
pyridine; chromium(VI) oxide; aluminum oxide; potassium hydroxide; sodium tetrahydroborate; sodium periodate; lithium aluminium tetrahydride; tributylphosphine; boron trifluoride diethyl etherate; methyllithium; hydrogen; sodium hydrogencarbonate; ozone;
palladium on activated charcoal;
In
tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; dichloromethane; water; benzene;