1-Butanesulfonic acid, trimethylsilyl ester

Base Information

• Chemical Name: 1-Butanesulfonic acid, trimethylsilyl ester
• CAS No.: 72500-12-0
• Molecular Formula: C7H18O3SSi
• Molecular Weight: 210.37
• Mol file: 72500-12-0.mol

Synonyms:

Chemical Property of 1-Butanesulfonic acid, trimethylsilyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Butanesulfonic acid, trimethylsilyl ester

There total 3 articles about 1-Butanesulfonic acid, trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

chloro-trimethyl-silane (75-77-4) + C6H9F3O4S (72500-13-1) → trifluoracetyl chloride (354-32-5) + Trimethylsilyl-1-butansulfonat (72500-12-0)

Guidance literature:

for 24h; Ambient temperature;

Reference yield: 83.5%

chloro-trimethyl-silane (75-77-4) + C6H12O4S → Trimethylsilyl-1-butansulfonat (72500-12-0) + acetyl chloride (75-36-5)

Guidance literature:

for 24h; Ambient temperature;

Reference yield: 72.0%

butane-1-sulfonic acid methyl ester (2374-69-8) + N-trimethylsilyl-pyrrolidin-2-one (14468-90-7) → 1-methyl-pyrrolidin-2-one (872-50-4,26138-58-9) + Trimethylsilyl-1-butansulfonat (72500-12-0)

Guidance literature:

Heating;

DOI:10.1007/s11172-020-2775-x

upstream raw materials:

chloro-trimethyl-silane

C₆H₉F₃O₄S

butane-1-sulfonic acid methyl ester

N-trimethylsilyl-pyrrolidin-2-one

Downstream raw materials:

1-butanesulfonic acid sodium salt

Refernces

• 1、 Shipov, A. G.,Baukov, Yu. I.. "α-(TRIALKYLSILYL)-, α-(TRIALKYLGERMYL)-, AND α-(TRIALKYLSTANNYL)-ALKANESULFONIC ESTERS AND AMIDES AND TRIMETHYLSILYL SULFONATES: THEIR SYNTHESIS AND SOME OF THEIR REACTIONS". . p. 1642 - 1657. Retrieved 2007/10/02.