Technology Process of 2,4-Di-tert-butyl-6-chloroaniline
There total 2 articles about 2,4-Di-tert-butyl-6-chloroaniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
nickel;
In
ethanol;
for 7h;
under 760 Torr;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) hydrochloric acid, sodium nitrite; 2.) cuprous chloride / 1.) glacial acetic acid, water, 0 deg C, 15 min; 2.) r.t., overnight
2: 55 percent / H2 / Raney nickel / ethanol / 7 h / 760 Torr
With
hydrogenchloride; hydrogen; copper(l) chloride; sodium nitrite;
nickel;
In
ethanol;
- Guidance literature:
-
With
sulfuric acid;
for 24h;
Ambient temperature;