2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate

Base Information

• Chemical Name: 2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate
• CAS No.: 7233-42-3
• Molecular Formula: C₂₈H₄₁N₃O₁₆
• Molecular Weight: 675.644
• Mol file: 7233-42-3.mol

Synonyms:

Chemical Property of 2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate

Chemical Property:

• Melting Point: 259 - 262 °C
• Boiling Point: 393.3°Cat760mmHg
• Flash Point: 191.7°C
• PSA: 62.44000
• Density: g/cm³
• LogP: 2.42870
• Solubility.: Chloroform, Methanol

Purity/Quality:

2,2''-Diacetamido-2,2''-dideoxy-di-β-D-glucopyranosylamine3,3'',4,4'',6,6''-Hexaacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: An amino sugar used in the preparation of N-acyl derivatives of 2-acetamido-2-deoxy-β-D-glucosylamine. 2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate is an amino sugar used in the preparation of N-acyl derivatives of 2-acetamido-2-deoxy-β-D-glucosylamine.

Technology Process of 2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate

There total 2 articles about 2,2'-DiacetaMido-2,2'-dideoxy-di-β-D-glucopyranosylaMine 3,3',4,4',6,6'-Hexaacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine (4515-24-6) + N-<2-(Triphenylphosphonio)ethoxycarbonyl>asparaginsaeure-1-tert-butylester-chlorid (86088-19-9) → 2-Acetamido-N-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosylamin (7233-42-3) + 2-Acetamido-N-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,4,6-tri-O-acetyl-2-desoxy-α-D-glucopyranosylamin (6205-70-5,7057-04-7,7233-42-3) + N4-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-N2-<2-(triphenylphosphonio)ethoxycarbonyl>asparagin-tert-butylester-chlorid (86088-20-2)

Guidance literature:

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In chloroform; for 15h; Ambient temperature;

DOI:10.1002/jlac.198319830302

Reference yield: 63.0%

2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine (4515-24-6) + N-<2-(Triphenylphosphonio)ethoxycarbonyl>asparaginsaeure-1-tert-butylester-chlorid (86088-19-9) → 2-Acetamido-N-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosylamin (7233-42-3) + 2-Acetamido-N-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,4,6-tri-O-acetyl-2-desoxy-α-D-glucopyranosylamin (6205-70-5,7057-04-7,7233-42-3) + N4-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-N2-<2-(triphenylphosphonio)ethoxycarbonyl>asparagin-tert-butylester-chlorid (86088-20-2)

Guidance literature:

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In chloroform; for 15h; Ambient temperature;

DOI:10.1002/jlac.198319830302

upstream raw materials:

2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

N-<2-(Triphenylphosphonio)ethoxycarbonyl>asparaginsaeure-1-tert-butylester-chlorid

Refernces