Perfluoro-2,5-diazahexane-2,5-dioxyl

Base Information

• Chemical Name: Perfluoro-2,5-diazahexane-2,5-dioxyl
• CAS No.: 36525-64-1
• Molecular Formula: C4F10 N2 O2
• Molecular Weight: 298.04
• Hs Code.: 2928009090
• Mol file: 36525-64-1.mol

Synonyms:Perfluoro-2,5-diazahexane-2,5-dioxyl;MFCD02093331;AKOS025310380;Perfluoro-2,5-diazahexane-2,5-dioxyl 97%;(Perfluoroethylene)bis[(perfluoromethyl)aminyl]dioxide

Chemical Property of Perfluoro-2,5-diazahexane-2,5-dioxyl

Chemical Property:

• Boiling Point: 119.4°Cat760mmHg
• Flash Point: 26°C
• PSA: 6.48000
• Density: 1.89g/cm³
• LogP: 2.50660
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 3
• Exact Mass: 297.98000887
• Heavy Atom Count: 18
• Complexity: 267

Purity/Quality:

99% ^*data from raw suppliers

Perfluoro-2,5-diazahexane-2,5-dioxyl 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(N(C(F)(F)F)[O])(F)F)(N(C(F)(F)F)[O])(F)F

Technology Process of Perfluoro-2,5-diazahexane-2,5-dioxyl

There total 1 articles about Perfluoro-2,5-diazahexane-2,5-dioxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ perfluoro-NN'-dimethylethane-1,2-bis(amino-oxyl) diradical (36525-64-1)

Guidance literature:

CF3*NO-C2F4-PCl3, 1) H2O, 2) KMnO4;

DOI:10.1039/C39720000833

Reference yield: 99.0%

bis(triphenylphosphine)iridium(I) carbonyl chloride (15318-31-7,14871-41-1,59246-46-7) + perfluoro-NN'-dimethylethane-1,2-bis(amino-oxyl) diradical (36525-64-1) → carbonylchloro[perfluoro-NN'-dimethylethane-1,2-bis(amino-oxy)]bis(triphenylphosphine)iridium(III)-benzene (1/1)

Guidance literature:

With benzene; In tetrachloromethane; addn. of diradical to Ir complex soln. in dried de-aerated CCl4, stirring for 15 min at 25°C under N2; vac. evapn., dissolving in benzene, addn. of methanol, elem. anal.;

DOI:10.1039/DT9820000671

Reference yield: 94.0%

tetrakis(triphenylphosphine)platinum (14221-02-4) + cyclohexane (110-82-7,25012-93-5) + perfluoro-NN'-dimethylethane-1,2-bis(amino-oxyl) diradical (36525-64-1) → [perfluoro-NN'-dimethylethane-1,2-bis(amino-oxy)]bis(triphenylphosphine)platinum(II)-cyclohexane (1/1)

Guidance literature:

In benzene; addn. of diradical to Pt complex soln. in dried de-aerated benzene withstirring over 15 min at 25°C under N2; recrystn. (CH2Cl2/cyclohexane), elem. anal.;

DOI:10.1039/DT9820000671

Downstream raw materials:

trifluoronitrosomethane

Perfluoro-2-azapropen

perfluoro(4,7-dimethyl-1,3-dioxa-2-tetrafluorothia-4,7-diazacycloheptane)

trifluoromethyl isocyanate