Technology Process of Dichloroethylsilane
There total 21 articles about Dichloroethylsilane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
ethyl bromide;
With
magnesium;
In
diethyl ether;
Reflux;
With
trichlorosilane;
In
diethyl ether;
at 15 ℃;
DOI:10.1134/S1070427214050164
- Guidance literature:
-
With
Si-Cu-Co;
In
neat (no solvent);
byproducts: (CH3)3SiCl, HSiCl3, SiCl4; C2H5Cl and Si-Cu-Co (88:10:2) activated with CuCl-CuCl2 at 340-360°C;;
- Guidance literature:
-
With
hydrogenchloride; silicon grains; copper(l) chloride;
at 259.84 ℃;
for 5h;
DOI:10.1039/b007068h