Aphylline

Base Information Edit

Chemical Name:Aphylline
CAS No.:577-37-7
Molecular Formula:C15H24N2O
Molecular Weight:248.3639
Hs Code.:
Mol file:577-37-7.mol

Synonyms:7,14-Methano-2H,6H-dipyrido[1,2-a:1‘,2‘-e][1,5]diazocin-6-one, dodecahydro-, [7R-(7-,7aα,14-,14a-)]-;

Suppliers and Price of Aphylline

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
APHYLLINE 95.00%
5MG
$ 501.69

Total 1 raw suppliers

Chemical Property of Aphylline Edit

Chemical Property:

Vapor Pressure:1.67E-06mmHg at 25°C
Melting Point:52-57°
Refractive Index:1.5286 (estimate)
Boiling Point:396.7°Cat760mmHg
Flash Point:172.7°C
PSA：23.55000
Density:1.16g/cm³
LogP:1.74750

Purity/Quality:

99% ^*data from raw suppliers

APHYLLINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Aphylline

There total 29 articles about Aphylline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: [7S-(7α,7aα,14α,14aβ)]-dodecahydro-7,14-methano-2H,6H-dihydro[1,2-a:1',2'-e]-[1,5]-diazocine sulphate

: 489-72-5,577-37-7,1218-51-5,6871-54-1,29882-72-2,82109-83-9,131829-31-7
(-)-17-oxosparteine

Guidance literature:: With sodium hydroxide; potassium hexacyanoferrate(III);
DOI:10.1515/znb-2002-0514

Reference yield: 69.0%

: 90-39-1,446-95-7,492-06-8,492-08-0,4985-24-4,6838-37-5,6917-37-9,24915-04-6,88269-31-2
sparteine

: 489-72-5,577-37-7,1218-51-5,6871-54-1,29882-72-2,82109-83-9,131829-31-7
17-oxosparteine

Guidance literature:: With DBN; oxygen; rose bengal; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Irradiation;
DOI:10.1021/acscatal.8b01897

Reference yield:

: 6376-21-2,7400-11-5,14691-01-1,18783-52-3,61740-19-0,76030-37-0
lupanine perchlorate

: 489-72-5,577-37-7,1218-51-5,6871-54-1,29882-72-2,82109-83-9,131829-31-7
17-oxosparteine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, / PtO₂, / aq. HCl / 15 h / 1034.3 Torr

2: 60 mg / potassium ferricyanide, 10percent NaOH, / aq. HCl / 0.67 h

With sodium hydroxide; hydrogen; potassium hexacyanoferrate(III); platinum(IV) oxide; In hydrogenchloride;
DOI:10.1139/v88-280