(butylsulfonyl)benzene

Base Information

• Chemical Name: (butylsulfonyl)benzene
• CAS No.: 16823-62-4
• Molecular Formula: C10H14 O2 S
• Molecular Weight: 198.286
• Mol file: 16823-62-4.mol

Synonyms:Sulfone,butyl phenyl (8CI); (Butylsulfonyl)benzene; 1-Phenylsulfonylbutane; Butylphenyl sulfone; NSC 42881; Phenyl butyl sulfone; n-Butyl Phenyl Sulfone

Chemical Property of (butylsulfonyl)benzene

Chemical Property:

• Vapor Pressure: 0.0002mmHg at 25°C
• Boiling Point: 337.8°Cat760mmHg
• Flash Point: 186.9°C
• Density: 1.097g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of (butylsulfonyl)benzene

There total 29 articles about (butylsulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(n-butylthio)benzene (1126-80-3) → butyl phenyl sulfone (16823-62-4)

Guidance literature:

With dihydrogen peroxide; titanium(IV) oxide; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1016/j.molcata.2010.03.011

Reference yield: 94.0%

1-iodo-butane (542-69-8) + PVS (5535-48-8) → butyl phenyl sulfone (16823-62-4)

Guidance literature:

PVS; With tetraethylammoniumcyanide; In dichloromethane; for 0.0833333h;

1-iodo-butane; In dichloromethane; at 20 ℃;

DOI:10.1055/s-0039-1690991

Reference yield: 90.0%

(n-butylthio)benzene (1126-80-3) → butyl phenyl sulfone (16823-62-4) + 1-(butylsulfinyl)benzene (13153-10-1)

Guidance literature:

With 1H-imidazole; tetra-n-butylammonium hydrogen monopersulfate; In dichloromethane; at 25 ℃; for 0.0333333h; chemoselective reaction;

DOI:10.1080/17415990903569551

upstream raw materials:

1-bromo-butane

sodium benzenesulfonate

(n-butylthio)benzene

methyl-phenyl-thioether

Downstream raw materials:

(4S)-tert-butyl-2-((2R,3S)-2-phenyl-3-phenylsulfonylhexyl)-oxazoline

butyric acid

[(4RS,7S)-7,11-dimethyldodec-10-en-4-yl](phenyl)sulfone

(4RS,7R)-7,11-dimethyldodec-10-en-4-yl(phenyl)sulfone

Refernces

• 1、 Baldwin,Robinson. "-". . p. 1445,1448. Retrieved 1932.
• 2、 Dhiman, Shefali. "Biocatalytic Oxidation of Sulfides to Sulfones". . p. 250 - 255. Retrieved 2021/03/29.
• 3、 Meng, Yingying,Wang, Ming,Jiang, Xuefeng. "Multicomponent Reductive Cross-Coupling of an Inorganic Sulfur Dioxide Surrogate: Straightforward Construction of Diversely Functionalized Sulfones". supporting information. p. 1346 - 1353. Retrieved 2019/12/11.