n-(4-Methylphenyl)-n-nitrosoformamide

Base Information

• Chemical Name: n-(4-Methylphenyl)-n-nitrosoformamide
• CAS No.: 22071-69-8
• Molecular Formula: C₈H₈N₂O₂
• Molecular Weight: 164.164
• NSC Number: 107564
• DSSTox Substance ID: DTXSID20944699
• Wikidata: Q82921938
• Mol file: 22071-69-8.mol

Synonyms:22071-69-8;n-(4-methylphenyl)-n-nitrosoformamide;NSC107564;DTXSID20944699;NSC-107564

Chemical Property of n-(4-Methylphenyl)-n-nitrosoformamide

Chemical Property:

• Vapor Pressure: 0.0072mmHg at 25°C
• Boiling Point: 269.6°Cat760mmHg
• Flash Point: 116.8°C
• Density: 1.15g/cm³
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 164.058577502
• Heavy Atom Count: 12
• Complexity: 164

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)N(C=O)N=O

Technology Process of n-(4-Methylphenyl)-n-nitrosoformamide

There total 2 articles about n-(4-Methylphenyl)-n-nitrosoformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-methylphenyl)formamide (3085-54-9) → formic acid-(N-nitroso-p-toluidide) (22071-69-8)

Guidance literature:

With mixture of gaseous nitrogen oxides; acetic acid;

Reference yield:

→ formic acid-(N-nitroso-p-toluidide) (22071-69-8)

Guidance literature:

Nitrosierung des Amins S. 584;

DOI:10.1039/J29710000583

Reference yield:

formic acid-(N-nitroso-p-toluidide) (22071-69-8) + phenylhydrazine (100-63-0) → 2-formyl-1-phenylhydrazine (622-84-4)

Guidance literature:

With benzene;

upstream raw materials:

N-(4-methylphenyl)formamide

Downstream raw materials:

2-formyl-1-phenylhydrazine

p-CH₃C₆H₄NNN(NH₂)C₆H₅