Glycarsamide

Base Information

• Chemical Name: Glycarsamide
• CAS No.: 144-87-6
• Molecular Formula: C8H10 As N O5
• Molecular Weight: 275.093
• Hs Code.: 2931900090
• European Community (EC) Number: 205-643-2
• NSC Number: 221701
• UNII: 3ACA67L6DG
• DSSTox Substance ID: DTXSID40162595
• Nikkaji Number: J193.644A
• Wikidata: Q27256967
• ChEMBL ID: CHEMBL1741842
• Mol file: 144-87-6.mol

Synonyms:Glycarsamide;144-87-6;4-(Glycolloylamino)phenylarsonic acid;N-Glycolylarsanilic acid;[4-[(2-hydroxyacetyl)amino]phenyl]arsonic acid;N-Glycoloylarsanilic acid;UNII-3ACA67L6DG;3ACA67L6DG;Arsanilic acid, N-glycoloyl-;p-Glycolylaminophenylarsinic acid;EINECS 205-643-2;NSC-221701;NSC163966;[4-[(HYDROXYACETYL)AMINO]PHENYL]ARSONIC ACID;NSC-163966;(4-((HYDROXYACETYL)AMINO)PHENYL)ARSONIC ACID;Astryl;GLYCARSAMIDE [MI];NCIStruc1_001581;NCIStruc2_001935;SCHEMBL225259;CHEMBL1741842;DTXSID40162595;p-Glycoloylaminophenylarsinic acid;p-Glycoloylaminophenylarsonic acid;p-Glycolylaminobenzenearsonic acid;p-Glycoloylaminobenzenearsonic acid;p-Hydroxyacetamidophenylarsonic acid;4-(glycolloylamino)phenylarsonicacid;4-(glycoloylamino)phenylarsonic acid;CCG-36631;MFCD00068960;NCGC00014459;NCI163966;NSC221701;AKOS023506036;NSC 221701;NCGC00014459-02;NCGC00097564-01;NCI60_001246;[4-(2-hydroxyacetamido)phenyl]arsonic acid;Arsonic acid, [4-[(hydroxyacetyl)amino]phenyl]-;Q27256967

Chemical Property of Glycarsamide

Chemical Property:

• Melting Point: 202-203°
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 106.86000
• Density: g/cm³
• LogP: -1.74860
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 274.977492
• Heavy Atom Count: 15
• Complexity: 268

Purity/Quality:

98%min ^*data from raw suppliers

Astryl ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1NC(=O)CO)[As](=O)(O)O

Technology Process of Glycarsamide

There total 7 articles about Glycarsamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-aminophenylarsonic acid (98-50-0) + glycolic Acid (79-14-1) → (4-glycoloylamino-phenyl)-arsonic acid (144-87-6)

Guidance literature:

With water; at 120 ℃;

Reference yield:

Gca-pNA (62100-58-7) → (4-glycoloylamino-phenyl)-arsonic acid (144-87-6)

Guidance literature:

With ethanol; nickel; at 70 - 80 ℃; Hydrogenation_.unter Druck und Behandlung des Reaktionsprodukts mit wss.Salzsaeure und Natriumnitrit und anschliessend mit alkal.wss.Natriumarsenit-Loesung;

Reference yield:

[4-(2-chloro-acetylamino)-phenyl]-arsonic acid (5425-62-7) → (4-glycoloylamino-phenyl)-arsonic acid (144-87-6)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

p-aminophenylarsonic acid

glycolic Acid

Gca-pNA

[4-(2-chloro-acetylamino)-phenyl]-arsonic acid