Technology Process of Acetic acid, [2-(5-phenyl-3-isoxazolyl)phenoxy]-, 2-acetylphenyl ester
There total 4 articles about Acetic acid, [2-(5-phenyl-3-isoxazolyl)phenoxy]-, 2-acetylphenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trichlorophosphate;
In
pyridine;
for 8h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydroxylamine hydrochloride / pyridine / Heating
2: 82 percent / potassium carbonate / acetone / Heating
3: 56 percent / ethanol; aq. NaOH / 2 h / Heating
4: 63 percent / phosphorus oxychloride / pyridine / 8 h / Ambient temperature
With
hydroxylamine hydrochloride; potassium carbonate; trichlorophosphate;
In
pyridine; sodium hydroxide; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / potassium carbonate / acetone / Heating
2: 56 percent / ethanol; aq. NaOH / 2 h / Heating
3: 63 percent / phosphorus oxychloride / pyridine / 8 h / Ambient temperature
With
potassium carbonate; trichlorophosphate;
In
pyridine; sodium hydroxide; ethanol; acetone;
