Technology Process of 2-Pentenoic acid, 3-methyl-, ethyl ester
There total 20 articles about 2-Pentenoic acid, 3-methyl-, ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyllithium;
With
copper(l) iodide;
In
tetrahydrofuran; diethyl ether;
at -35 - -20 ℃;
Inert atmosphere;
ethyl pent-2-ynoate;
In
tetrahydrofuran; diethyl ether;
at -78 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol801940r
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium cyanoborohydride; triphenylphosphine;
In
tetrahydrofuran;
at 60 ℃;
for 15h;
DOI:10.1021/jo00369a043
