Technology Process of 11-[5-[[5-Cyano-2-(2,6-dimethylmorpholin-4-yl)-1-ethyl-4-methyl-6-oxopyridin-3-yl]methylidene]-4-oxo-2-sulfanylidene-1,3-thiazolidin-3-yl]undecanoic acid
There total 20 articles about 11-[5-[[5-Cyano-2-(2,6-dimethylmorpholin-4-yl)-1-ethyl-4-methyl-6-oxopyridin-3-yl]methylidene]-4-oxo-2-sulfanylidene-1,3-thiazolidin-3-yl]undecanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran; benzene;
at 5 - 10 ℃;
for 2h;
Product distribution;
other organomagnesium compound, other solvents;
DOI:10.1055/s-1980-29247
- Guidance literature:
-
acetone;
With
N–nitrosuccinimide; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate;
at 20 ℃;
for 4h;
Inert atmosphere;
Irradiation;
phenylacetylene;
at 20 ℃;
for 8h;
Inert atmosphere;
Irradiation;
DOI:10.1002/chem.201902966
- Guidance literature:
-
With
hydrogenchloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium nitrite;
In
water; N,N-dimethyl-formamide;
at 120 ℃;
for 24h;
DOI:10.1002/ejoc.202101411
