Ethanone, 1-(2-hydroxy-5-nonylphenyl)-, oxime

Base Information

• Chemical Name: Ethanone, 1-(2-hydroxy-5-nonylphenyl)-, oxime
• CAS No.: 59344-62-6
• Molecular Formula: C17H27NO2
• Molecular Weight: 277.407
• Hs Code.: 2928000090
• Mol file: 59344-62-6.mol

Synonyms:SME 530;LIX 84I;Ethanone,1-(2-hydroxy-5-nonylphenyl)-,oxime;SME 529;Shell 529;MOC 45;

Chemical Property of Ethanone, 1-(2-hydroxy-5-nonylphenyl)-, oxime

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.513
• Boiling Point: 425.864 °C at 760 mmHg
• PKA: 9.35±0.50(Predicted)
• Flash Point: 276.572 °C
• PSA: 52.82000
• Density: 1.008g/cm³
• LogP: 4.88350

Purity/Quality:

99% ^*data from raw suppliers

1-(2-Hydroxy-5-nonylphenyl)ethanoneoxime 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(2-hydroxy-5-nonylphenyl)-, oxime

There total 3 articles about Ethanone, 1-(2-hydroxy-5-nonylphenyl)-, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-hydroxy-5-nonylacetophenone (115851-77-9) → 2-hydroxy-5-nonylacetophenone oxime (59344-62-6)

Guidance literature:

With isooctanoic acid; hydroxylamine hydrochloride; sodium carbonate; In water; toluene; at 70 ℃; for 4h; Temperature; Microwave irradiation;

Reference yield:

→ 2-hydroxy-5-nonylacetophenone oxime (59344-62-6)

Guidance literature:

With sodium carbonate; hydroxylamine sulfate; In Octanoic acid; water; at 70 ℃; for 4.5h;

Reference yield:

4-Nonylphenol (104-40-5) → 2-hydroxy-5-nonylacetophenone oxime (59344-62-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogen sulfate / 3 h / Reflux

2: silica gel-supported solid composite chloride salt / hexane / 0.02 h / Microwave irradiation

3: isooctanoic acid; hydroxylamine hydrochloride; sodium carbonate / toluene; water / 4 h / 70 °C / Microwave irradiation

With sodium hydrogen sulfate; isooctanoic acid; hydroxylamine hydrochloride; sodium carbonate; In hexane; water; toluene;

upstream raw materials:

2-hydroxy-5-nonylacetophenone

4-Nonylphenol

Refernces

• 1、 -. "Ketoximes, processes therefor, and copper extraction process". Page column 11-12. . Retrieved 2008/06/13.