Acetone diethyl hydrazone

Base Information

• Chemical Name: Acetone diethyl hydrazone
• CAS No.: 16713-36-3
• Molecular Formula: C₇H₁₆N₂
• Molecular Weight: 128.217
• Hs Code.: 2928000090
• Mol file: 16713-36-3.mol

Synonyms:2-Propanone diethyl hydrazone;Acetone diethyl hydrazone

Chemical Property of Acetone diethyl hydrazone

Chemical Property:

• PSA: 15.60000
• LogP: 1.72400

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetone diethyl hydrazone

There total 4 articles about Acetone diethyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.2%

1-ethyl-2-(propan-2-ylidene)hydrazine (7422-99-3) + 1,1-diethyldiazenium bromide → aldehyde diethylhydrazone (7422-91-5) + tetraethyl-2-tetrazene (13304-29-5) + Aceton-diaethylhydrazon (16713-36-3) + 3,3-dimethyl-1,5,5-triethyl-3,4-dihydroformazan

Guidance literature:

With triethylamine; at -30 - -20 ℃; Further byproducts given. Title compound not separated from byproducts;

Reference yield: 30.2%

1-ethyl-2-(propan-2-ylidene)hydrazine (7422-99-3) + 1,1-diethyldiazenium bromide → tetraethyl-2-tetrazene (13304-29-5) + 3-methyl-1,5,5-triethyl-3,4-dihydroformazan (51576-32-0) + Aceton-diaethylhydrazon (16713-36-3) + 3,3-dimethyl-1,5,5-triethyl-3,4-dihydroformazan

Guidance literature:

With triethylamine; at -30 - -20 ℃; Further byproducts given. Title compound not separated from byproducts;

Reference yield:

N,N-diethylhydrazine (616-40-0) + acetone (67-64-1) → Aceton-diaethylhydrazon (16713-36-3)

Guidance literature:

upstream raw materials:

N,N-diethylhydrazine

acetone

1-ethyl-2-(propan-2-ylidene)hydrazine

Refernces