CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE

Base Information

• Chemical Name: CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE
• CAS No.: 626213-24-9
• Molecular Formula: C12H19NO
• Molecular Weight: 193.29
• Hs Code.: 2932190090
• Mol file: 626213-24-9.mol

Synonyms:CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE

Chemical Property of CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE

Chemical Property:

• PSA: 25.17000
• LogP: 3.40120

Purity/Quality:

98%min ^*data from raw suppliers

Cyclohexyl-(5-methyl-furan-2-ylmethyl)-amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE

There total 3 articles about CYCLOHEXYL-(5-METHYL-FURAN-2-YLMETHYL)-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Methylfurfural (620-02-0) + 1-nitrocyclohexane (1122-60-7) → cyclohexyl-(5-methyl-furfuryl)-amine (626213-24-9) + C12H17NO2 + C12H17NO + 2-hydroxymethyl-5-methylfuran (3857-25-8)

Guidance literature:

With 0.2 % Pt/C; hydrogen; In toluene; at 39.84 ℃; for 24h; under 3750.38 Torr; Reagent/catalyst; chemoselective reaction; Catalytic behavior;

DOI:10.1016/S1872-2067(16)62493-2

Reference yield:

2-methylfuran (534-22-5) + cyclohexylamine hydrochloride (4998-76-9) → cyclohexyl-(5-methyl-furfuryl)-amine (626213-24-9)

Guidance literature:

With formaldehyd;

DOI:10.1021/ja01211a017

Reference yield:

5-Methylfurfural (620-02-0) + 1-nitrocyclohexane (1122-60-7) → cyclohexyl-(5-methyl-furfuryl)-amine (626213-24-9) + C12H17NO2 + C12H17NO

Guidance literature:

With gold supported on titanium dioxide; hydrogen; In toluene; at 59.84 ℃; for 9h; under 7500.75 Torr; Solvent; Reagent/catalyst; chemoselective reaction; Catalytic behavior;

DOI:10.1016/S1872-2067(16)62493-2

upstream raw materials:

2-methylfuran

cyclohexylamine hydrochloride

5-Methylfurfural

1-nitrocyclohexane

Refernces