3-(Dichloro(methyl)silyl)propyl acetate

Base Information

• Chemical Name: 3-(Dichloro(methyl)silyl)propyl acetate
• CAS No.: 5290-24-4
• Molecular Formula: C6H12Cl2O2Si
• Molecular Weight: 215.152
• Hs Code.: 2931900090
• European Community (EC) Number: 226-126-8
• DSSTox Substance ID: DTXSID80967369
• Nikkaji Number: J297.979I
• Wikidata: Q72434400
• Mol file: 5290-24-4.mol

Synonyms:5290-24-4;3-(Dichloro(methyl)silyl)propyl acetate;3-[dichloro(methyl)silyl]propyl acetate;3-ACETOXYPROPYL METHYL DICHLOROSILANE;3-(Dichloromethylsilyl)propyl acetate;3-ACETOXYPROPYLMETHYLDICHLOROSILANE;1-Propanol, 3-(dichloromethylsilyl)-, acetate;EINECS 226-126-8;1-Propanol, 3-(dichloromethylsilyl)-, 1-acetate;ACETOXYPROPYLMETHYLDICHLOROSILANE;C6H12Cl2O2Si;SCHEMBL524942;C6-H12-Cl2-O2-Si;DTXSID80967369;3-Acetoxypropyldichloro(methyl)silane;MFCD00053905;AKOS022171983;FT-0698537

Chemical Property of 3-(Dichloro(methyl)silyl)propyl acetate

Chemical Property:

• Vapor Pressure: 0.13mmHg at 25°C
• Melting Point: <0°C
• Refractive Index: 1.4434
• Boiling Point: 224.8 °C at 760 mmHg
• Flash Point: 89.7 °C
• PSA: 26.30000
• Density: 1.134g/cm³
• LogP: 2.48920
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 213.9983615
• Heavy Atom Count: 11
• Complexity: 139

Purity/Quality:

98% ^*data from raw suppliers

3-ACETOXYPROPYL METHYL DICHLOROSILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCCC[Si](C)(Cl)Cl

Technology Process of 3-(Dichloro(methyl)silyl)propyl acetate

There total 3 articles about 3-(Dichloro(methyl)silyl)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichloromethylsilane (75-54-7) + Allyl acetate (591-87-7) → (3-acetoxy-propyl)-dichloro-methyl-silane (5290-24-4)

Guidance literature:

With dicyclohexyl peroxydicarbonate;

Reference yield:

Dichloromethylsilane (75-54-7) + Allyl acetate (591-87-7) → (3-acetoxy-propyl)-dichloro-methyl-silane (5290-24-4) + C3H6Cl2O2Si (37170-31-3)

Guidance literature:

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In toluene; at 40 - 60 ℃; for 16h; Overall yield = 92 %Spectr.;

DOI:10.1016/j.jcat.2012.06.006

Reference yield:

→ (3-acetoxy-propyl)-dichloro-methyl-silane (5290-24-4)

Guidance literature:

/BRN= 1779054/;

DOI:10.1021/ja01561a054

upstream raw materials:

Dichloromethylsilane

Allyl acetate

Downstream raw materials:

3-trimethylsilyl-1-propanol

Refernces