methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate

Base Information Edit

Chemical Name:methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate
CAS No.:870837-20-0
Molecular Formula:C13H15NO5
Molecular Weight:265.266
Hs Code.:
Mol file:870837-20-0.mol

Synonyms:methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate;methyl 3-methoxy-4-(N-(2-oxopropyl)formamido)benzoate

Suppliers and Price of methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate Edit

Chemical Property:

Boiling Point:455.4±45.0 °C(Predicted)
PKA:-1.35±0.50(Predicted)
PSA：72.91000
Density:1.223±0.06 g/cm3(Predicted)
LogP:1.66950

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate

There total 5 articles about methyl 4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 64-18-6
formic acid

: 41608-64-4
methyl 3-methoxy-4-aminobenzoate

: 78-95-5
chloroacetone

: 870837-20-0
4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoic acid methyl ester

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1021/acs.joc.6b02979

Reference yield:

: 700834-18-0
4-formylamino-3-methoxybenzoic acid methyl ester

: 78-95-5
chloroacetone

: 870837-20-0
4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoic acid methyl ester

Guidance literature:: With caesium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

Reference yield:

: 5081-37-8
methyl 3-methoxy-4-nitrobenzoate

: 870837-20-0
4-[formyl-(2-oxopropyl)amino]-3-methoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / methanol

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere

With hydrogen; potassium carbonate; potassium iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.6b02979