2-(3-BroMophenyl)-9H-BroMophenylcarbazole

Base Information

• Chemical Name: 2-(3-BroMophenyl)-9H-BroMophenylcarbazole
• CAS No.: 1365118-41-7
• Molecular Formula: C24H15Br2N
• Molecular Weight: 477.1906
• Mol file: 1365118-41-7.mol

Synonyms:2-(3-BroMophenyl)-9H-BroMophenylcarbazole;9H-Carbazole,2-(3-broMophenyl)-9-phenyl-;2-(3-Bromophenyl)-9-phenyl-9H-carbazole

Chemical Property of 2-(3-BroMophenyl)-9H-BroMophenylcarbazole

Chemical Property:

• Melting Point: 148.0 to 152.0 °C
• Boiling Point: 552.6±32.0 °C(Predicted)
• PSA: 4.93000
• Density: 1.32±0.1 g/cm3(Predicted)
• LogP: 7.21320
• Solubility.: soluble in Toluene

Purity/Quality:

99.0% ^*data from raw suppliers

2-(3-Bromophenyl)-9-phenylcarbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-BroMophenyl)-9H-BroMophenylcarbazole

There total 9 articles about 2-(3-BroMophenyl)-9H-BroMophenylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1,3-dibromobenzene (108-36-1) + 9-(phenyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole (1246669-45-3) → 2-(3-bromophenyl)-9-phenyl-9H-carbazole (1365118-41-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃;

Reference yield: 48.0%

1,3-dibromobenzene (108-36-1) + (9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid (1001911-63-2) → 2-(3-bromophenyl)-9-phenyl-9H-carbazole (1365118-41-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; for 24h; Reflux;

Reference yield:

1-Bromo-3-iodobenzene (591-18-4) + 9-(phenyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole (1246669-45-3) → 2-(3-bromophenyl)-9-phenyl-9H-carbazole (1365118-41-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; Reflux;

upstream raw materials:

4-bromo-2-nitro-1-phenylbenzene

2-bromo-9H-carbazole

9-(phenyl)-2-bromo-9H-carbazole

1,3-dibromobenzene

Refernces

• 1、 -. "COMPOUND FOR ORGANIC ELECTRONIC ELEMENT, ORGANIC ELECTRONIC ELEMENT USING SAME, AND ELECTRONIC DEVICE THEREWITH". . . Retrieved 2015/11/03.
• 2、 -. "NOVEL COMPOUNG FOR ORGANIC ELECTROLUMINESCENT DEVICE, ORGANIC ELECTROLUMINESCENT DEVICE INCLUDING THE SAME AND ELECTRIC APPARATUS". Paragraph 0165-0170. . Retrieved 2016/11/17.