Hexa(cyclohexyl)ditin

Base Information

• Chemical Name: Hexa(cyclohexyl)ditin
• CAS No.: 3047-10-7
• Molecular Formula: C36H66Sn2
• Molecular Weight: 736.34
• Hs Code.: 2931900090
• NSC Number: 227371
• Mol file: 3047-10-7.mol

Synonyms:HEXA(CYCLOHEXYL)DITIN;3047-10-7;1,1,1,2,2,2-Hexacyclohexyldistannane;Distannane, 1,1,1,2,2,2-hexacyclohexyl-;NSC227371;hexacyclohexyldistannan;AKOS025293660;NSC-227371

Chemical Property of Hexa(cyclohexyl)ditin

Chemical Property:

• Melting Point: >300°C
• PSA: 0.00000
• LogP: 12.96820
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 6
• Exact Mass: 736.32026
• Heavy Atom Count: 38
• Complexity: 457

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)[Sn](C2CCCCC2)C3CCCCC3.C1CCC(CC1)[Sn](C2CCCCC2)C3CCCCC3

Technology Process of Hexa(cyclohexyl)ditin

There total 6 articles about Hexa(cyclohexyl)ditin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

tricyclohexyltin hydride (6056-50-4) + 1-docosene (1599-67-3) → tricyclohexyldocosyltin (958632-61-6) + hexacyclohexylditin (3047-10-7)

Guidance literature:

With azobis(isobutyronitrile); In neat (no solvent); (N2); using Schlenk techniques; heating of docos-1-ene with SnCy3H in the presence of azobis(isobutyronitrile) at 110°C;

DOI:10.1021/om700534j

Reference yield:

→ hexacyclohexylditin (3047-10-7)

Guidance literature:

With sodium; xylene;

Reference yield:

tris(cyclohexyl)tin bromide (3023-92-5) → hexacyclohexylditin (3047-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: not given

In diethyl ether;

upstream raw materials:

cyclohexylmagnesiumchloride

cyclohexylmagnesium bromide

tricyclohexyltin hydride

(cyclo-C₆H₁₁)3SnN(C₂H₅)2

Downstream raw materials:

tris(cyclohexyl)(phenyl)stannane

Refernces