Technology Process of 3-Chloro-2,2-dimethylpropanamide
There total 4 articles about 3-Chloro-2,2-dimethylpropanamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia;
In
dichloromethane;
at 20 ℃;
for 2.75h;
Cooling with ice;
- Guidance literature:
-
With
ammonium cerium (IV) nitrate;
In
water; acetonitrile;
at 0 ℃;
for 2h;
DOI:10.1002/ejoc.201600600
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; [bis(acetoxy)iodo]benzene / 16 h / 90 °C / Inert atmosphere; Sealed tube
2: dichloro bis(acetonitrile) palladium(II); trifluoroacetic acid; N-chloro-succinimide / 1,4-dioxane / 16 h / 25 °C / Inert atmosphere; Sealed tube
3: ammonium cerium (IV) nitrate / acetonitrile; water / 2 h / 0 °C
With
dichloro bis(acetonitrile) palladium(II); N-chloro-succinimide; ammonium cerium (IV) nitrate; [bis(acetoxy)iodo]benzene; palladium diacetate; trifluoroacetic acid;
In
1,4-dioxane; water; acetonitrile;
DOI:10.1002/ejoc.201600600
