Technology Process of (S)-methyl-2-acetamido-6-[2-(4-nitrobenzamido)benzamido]hexanoate
There total 5 articles about (S)-methyl-2-acetamido-6-[2-(4-nitrobenzamido)benzamido]hexanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide;
In
1,2-dichloro-ethane;
at 25 ℃;
for 24h;
DOI:10.1021/ja406383h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / water; acetone / 11 h / 0 - 20 °C
2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide / 1,2-dichloro-ethane / 24 h / 25 °C
With
sodium azide; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide;
In
water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ja406383h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / tetrahydrofuran / 2.5 h / 0 - 20 °C
2: thionyl chloride / 0 °C
3: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide / 1,2-dichloro-ethane / 24 h / 25 °C
With
thionyl chloride; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium hydroxide; silver(I) triflimide;
In
tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ja406383h
