2-Furancarbonyl bromide (9CI)

Base Information

• Chemical Name: 2-Furancarbonyl bromide (9CI)
• CAS No.: 58777-49-4
• Molecular Formula: C₅H₃BrO₂
• Molecular Weight: 174.982
• Mol file: 58777-49-4.mol

Synonyms:2-Furoylbromide

Chemical Property of 2-Furancarbonyl bromide (9CI)

Chemical Property:

• Vapor Pressure: 0.561mmHg at 25°C
• Boiling Point: 189.7°Cat760mmHg
• Flash Point: 68.6°C
• PSA: 30.21000
• Density: 1.742g/cm³
• LogP: 1.81470

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Furancarbonyl bromide (9CI)

There total 2 articles about 2-Furancarbonyl bromide (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-furyl)-1-ethanone (1192-62-7,80145-44-4) → 2-furoyl bromide (58777-49-4) + rac-1-(2-furyl)-2-(methylamino)ethanol (2745-40-6)

Guidance literature:

With ammonium chloride; bromine; In 1,4-dioxane; diethyl ether;

Reference yield:

2-furanoic acid (88-14-2) → 2-furoyl bromide (58777-49-4)

Guidance literature:

With phosphorus tribromide;

DOI:10.1002/hlca.193401701138

Reference yield:

2-furoyl bromide (58777-49-4) + cyclohexylamine (108-91-8,157973-60-9) → N-cyclohexylfuran-2-carboxamide (10354-47-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2006.06.013

upstream raw materials:

2-furanoic acid

1-(2-furyl)-1-ethanone

Downstream raw materials:

N-cyclohexylfuran-2-carboxamide

Refernces

• 1、 -. "Pyridoquinoxaline antivirals". . . Retrieved 2008/06/13.