E-4-N,N-dimethylaminobenzaldoxime

Base Information

• Chemical Name: E-4-N,N-dimethylaminobenzaldoxime
• CAS No.: 57678-40-7
• Molecular Formula: C₉H₁₂N₂O
• Molecular Weight: 164.207
• Mol file: 57678-40-7.mol

Synonyms:E-4-N,N-dimethylaminobenzaldoxime

Chemical Property of E-4-N,N-dimethylaminobenzaldoxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of E-4-N,N-dimethylaminobenzaldoxime

There total 4 articles about E-4-N,N-dimethylaminobenzaldoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-(dimethylamino)benzaldehyde (579-72-6) → E-4-N,N-dimethylaminobenzaldoxime (57678-40-7)

Guidance literature:

With hydrogenchloride; hydroxylamine hydrochloride; potassium carbonate; In ethanol; water; at 60 ℃; for 0.0666667h; pH=10; Sonication;

Reference yield:

2-(dimethylamino)benzaldehyde (579-72-6) → 2-dimethylamino-benzaldehyde-oxime (57678-40-7)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride;

Reference yield:

anthranil (271-58-9) → 2-dimethylamino-benzaldehyde-oxime (57678-40-7)

Guidance literature:

Multi-step reaction with 2 steps

2: NaOH-solution; hydroxylamine hydrochloride

With sodium hydroxide; hydroxylamine hydrochloride;

upstream raw materials:

2-(dimethylamino)benzaldehyde

anthranil

o-aminobenzaldehyde

Downstream raw materials:

(2-Dimethylamino-benzyl)-(2,4-dinitro-phenyl)-amine

2-Chloro-N-(2-dimethylamino-benzyl)-acetamide

2-(aminomethyl)phenyl-N,N-dimethylamine

Refernces