C₄₅H₄₅NO₁₆

Base Information

• Chemical Name: C₄₅H₄₅NO₁₆
• CAS No.: 124667-86-3
• Molecular Formula: C₄₅H₄₅NO₁₆
• Molecular Weight: 855.849
• Mol file: 124667-86-3.mol

Synonyms:C₄₅H₄₅NO₁₆

Chemical Property of C₄₅H₄₅NO₁₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₄₅H₄₅NO₁₆

There total 2 articles about C₄₅H₄₅NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

normorphine (466-97-7,13396-02-6,99295-16-6,142864-36-6) → C45H45NO16 (124667-86-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 790 mg / 5percent NaHCO₃

2: Ag₂CO₃ / benzene / 30 h / Heating

With sodium hydrogencarbonate; silver carbonate; In benzene;

DOI:10.1248/cpb.37.955

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → C45H45NO16 (124667-86-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 790 mg / 5percent NaHCO₃

2: Ag₂CO₃ / benzene / 30 h / Heating

With sodium hydrogencarbonate; silver carbonate; In benzene;

DOI:10.1248/cpb.37.955

Reference yield:

C45H45NO16 (124667-86-3) → normorphin-6-yl-β-D-glucopyranosiduronate (NM-6-G) (65060-95-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd-C / methanol; CHCl₃

2: NaOMe

3: 0.43 N Ba(OH)2 / 2 h

With barium dihydroxide; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; chloroform;

DOI:10.1248/cpb.37.955

upstream raw materials:

normorphine

benzyl chloroformate

Downstream raw materials:

normorphin-6-yl-β-D-glucopyranosiduronate (NM-6-G)

Refernces