trifluoromethyl-arsonous acid diiodide

Base Information

• Chemical Name: trifluoromethyl-arsonous acid diiodide
• CAS No.: 353-91-3
• Molecular Formula: CAsF₃I₂
• Molecular Weight: 397.737
• Mol file: 353-91-3.mol

Synonyms:trifluoromethyl-arsonous acid diiodide

Chemical Property of trifluoromethyl-arsonous acid diiodide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of trifluoromethyl-arsonous acid diiodide

There total 5 articles about trifluoromethyl-arsonous acid diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

tris(trifluoromethyl)arsine (432-02-0) → iodotrifluoromethane (2314-97-8,263005-66-9) + trifluoromethyl-arsonous acid diiodide (353-91-3) + iodo-bis-trifluoromethyl-arsine (359-55-7)

Guidance literature:

100-105°C, 72 h;

Reference yield: 8.0%

tris(trifluoromethyl)arsine (432-02-0) + iodine (7553-56-2,12190-71-5,8031-47-8) → iodotrifluoromethane (2314-97-8,263005-66-9) + trifluoromethyl-arsonous acid diiodide (353-91-3) + iodo-bis-trifluoromethyl-arsine (359-55-7) + arsenic triiodide (7784-45-4)

Guidance literature:

100°C, 48 h; at high temp. more AsI3 and CF3I;

Reference yield:

arsenic + iodotrifluoromethane (2314-97-8,263005-66-9) → trifluoromethyl-arsonous acid diiodide (353-91-3) + iodo-bis-trifluoromethyl-arsine (359-55-7) + tris(trifluoromethyl)arsine (432-02-0) + arsenic triiodide (7784-45-4)

Guidance literature:

In neat (no solvent); on heating in sealing tube to 220-240°C; mechanism discussed;;

upstream raw materials:

tris(trifluoromethyl)arsine

iodine

arsenic triiodide

iodotrifluoromethane

Downstream raw materials:

tristrifluoromethylarsine

trifluoromethyldichloroarsine

Pentakis(trifluormethyl)-cyclopentaarsan

tetrakis(trifluoromethyl) cyclotetraarsane