Technology Process of C30H44O4Si
There total 7 articles about C30H44O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-ethynyl-4-(benzyloxy)-3-methoxybenzene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
Inert atmosphere;
(3S)-3-{[1-(tert-butyl)-1,1-dimethylsilyl]oxy}octanal;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 4h;
With
ammonium chloride;
In
tetrahydrofuran; hexane;
DOI:10.1016/j.tetasy.2011.11.010
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium periodate / tetrahydrofuran; water / 1 h
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
2.2: 4 h / -78 - 20 °C
With
sodium periodate; n-butyllithium;
In
tetrahydrofuran; hexane; water;
DOI:10.1016/j.tetasy.2011.11.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 20 °C
2.1: sodium periodate / tetrahydrofuran; water / 1 h
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
3.2: 4 h / -78 - 20 °C
With
sodium periodate; osmium(VIII) oxide; n-butyllithium; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; hexane; water; acetone; toluene;
DOI:10.1016/j.tetasy.2011.11.010