dibutyl phosphorochloridodithioite

Base Information

• Chemical Name: dibutyl phosphorochloridodithioite
• CAS No.: 28896-77-7
• Molecular Formula: C₈H₁₈ClPS₂
• Molecular Weight: 244.79
• Mol file: 28896-77-7.mol

Synonyms:dibutyl phosphorochloridodithioite

Chemical Property of dibutyl phosphorochloridodithioite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibutyl phosphorochloridodithioite

There total 2 articles about dibutyl phosphorochloridodithioite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

merphos (150-50-5) → dibutyl disulfide (629-45-8) + dibutyl phosphorochloridodithioite (28896-77-7) + dibutyl (trichloromethyl)phosphonodithioite

Guidance literature:

With tetrachloromethane; at 110 - 120 ℃; for 40h;

Reference yield:

tetrachloromethane (56-23-5) + merphos (150-50-5) → dibutyl disulfide (629-45-8) + dibutyl phosphorochloridodithioite (28896-77-7) + dibutyl (trichloromethyl)phosphonodithioite

Guidance literature:

at 110 - 120 ℃; for 40h;

Reference yield: 55.5%

dibutyl phosphorochloridodithioite (28896-77-7) + N,N-bis(trimethylsilyl)acetamide (10416-58-7) → chloro-trimethyl-silane (75-77-4) + S,S'-di(n-butyl) trimethylsilyl dithiophosphite (118467-51-9) + acetonitrile (75-05-8,26809-02-9)

Guidance literature:

Heating;

DOI:10.1007/BF00957268

upstream raw materials:

tetrachloromethane

merphos

Downstream raw materials:

merphos

Dichlorobutylthiophosphite

chloro-trimethyl-silane

S,S'-di(n-butyl) trimethylsilyl dithiophosphite

Refernces