1,2-Bis(4-nitrophenyl)ethane

Base Information Edit

Chemical Name:1,2-Bis(4-nitrophenyl)ethane
CAS No.:736-30-1
Molecular Formula:C14H12N2O4
Molecular Weight:272.26
Hs Code.:29042000
European Community (EC) Number:212-001-5
NSC Number:60022,608
UNII:SY1ZK3A4XO
DSSTox Substance ID:DTXSID2061066
Nikkaji Number:J193.106G
Wikidata:Q27115767
Mol file:736-30-1.mol

Synonyms:4,4'-Dinitrobibenzyl;1,2-Bis(4-nitrophenyl)ethane;736-30-1;4,4'-Dinitrodibenzyl;p,p'-Dinitrodibenzyl;1,2-Bis(p-nitrophenyl)ethane;p,p'-Dinitrobibenzyl;1-Nitro-4-[2-(4-nitrophenyl)ethyl]benzene;Bibenzyl, 4,4'-dinitro-;NSC 608;1,2-Ethanediylbis(4-nitrobenzene);1,1'-(1,2-Ethanediyl)bis(4-nitrobenzene);NSC 60022;Benzene, 1,1'-(1,2-ethanediyl)bis[4-nitro-;Dinitro-4,4' dibenzyle [French];Dinitro-4,4' dibenzyle;EINECS 212-001-5;UNII-SY1ZK3A4XO;Benzene, 1,1'-(1,2-ethanediyl)bis(4-nitro-;SY1ZK3A4XO;NSC-608;NSC-60022;Bibenzyl,4'-dinitro-;EC 212-001-5;1,2-Ethanediylbis[4-nitrobenzene];Benzene,1'-(1,2-ethanediyl)bis[4-nitro-;p,p'-Dinitro-bibenzyl;BIS(P-NITROBENZYL);Benzene,1,1'-(1,2-ethanediyl)bis[4-nitro-;NCIOpen2_002512;NSC608;SCHEMBL3292782;DTXSID2061066;CHEBI:34040;4,4'-DINITRODIHYDROSTILBENE;AMY18600;NSC60022;MFCD00014719;STK005038;AKOS003063993;LS-30245;1,1'-ethane-1,2-diylbis(4-nitrobenzene);A9489;FT-0606314;1-nitro-4-[2-(4-nitrophenyl)-ethyl]-benzene;1-Nitro-4-[2-(4-nitrophenyl)ethyl]benzene #;Q27115767

Suppliers and Price of 1,2-Bis(4-nitrophenyl)ethane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4,4'-DINITROBIBENZYL Aldrich
250mg
$ 144.00

Crysdot
1,2-Bis(4-nitrophenyl)ethane 95+%
1g
$ 460.00

American Custom Chemicals Corporation
4,4'-DINITROBIBENZYL 95.00%
5G
$ 1121.80

American Custom Chemicals Corporation
4,4'-DINITROBIBENZYL 95.00%
1G
$ 685.21

Alichem
1,2-Bis(4-nitrophenyl)ethane
1g
$ 409.20

Total 22 raw suppliers

Chemical Property of 1,2-Bis(4-nitrophenyl)ethane Edit

Chemical Property:

Appearance/Colour:solid
Vapor Pressure:0.001Pa at 20℃
Melting Point:179-183 °C(lit.)
Refractive Index:1.6180 (estimate)
Boiling Point:435 °C at 760 mmHg
Flash Point:208.4 °C
PSA：91.64000
Density:1.317 g/cm³
LogP:4.33460
Storage Temp.:2-8°C
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:272.07970687
Heavy Atom Count:20
Complexity:300

Purity/Quality:

99.9% ^*data from raw suppliers

4,4'-DINITROBIBENZYL Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 20/21/22
Safety Statements: 36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CCC2=CC=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1,2-Bis(4-nitrophenyl)ethane

There total 98 articles about 1,2-Bis(4-nitrophenyl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 99-99-0
1-methyl-4-nitrobenzene

: 736-30-1
1,2-bis(4-nitrophenyl)ethane

: 619-93-2,736-31-2,2501-02-2,101977-35-9
4,4'-dinitro stilbene

: 62-23-7
4-nitro-benzoic acid

Guidance literature:: With potassium hydroxide; 18-crown-6 ether; oxygen; In 1,2-dimethoxyethane; at 20 ℃; for 3.5h; under 760 Torr; other bases, other phase-transfer agents;
DOI:10.1007/BF00954087

Reference yield: 88.0%

: 100-14-1
4-nitrobenzyl chloride

: 736-30-1
1,2-bis(4-nitrophenyl)ethane

Guidance literature:: With 1-dodecyl-3-methylimidazolium cuprous chloride; copper; zinc; at 70 ℃; for 2.5h;
DOI:10.1007/s10562-010-0535-5

Reference yield: 80.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 100-14-1
4-nitrobenzyl chloride

: 736-30-1
1,2-bis(4-nitrophenyl)ethane

: 22865-59-4
Methyl 4-(4-Nitrobenzyl)phenyl Ether

Guidance literature:: With cis,cis,cis-tetrakis[(diphenylphosphanyl)methyl]cyclopentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); In xylene; at 130 ℃; for 20h;
DOI:10.1055/s-2003-40994