(2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine

Base Information

• Chemical Name: (2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine
• CAS No.: 53662-51-4
• Molecular Formula: C₆H₁₅N*C₈H₉NOS₂
• Molecular Weight: 300.489
• Mol file: 53662-51-4.mol

Synonyms:(2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine

Chemical Property of (2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine

There total 1 articles about (2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-phenylamine (90-04-0) + triethylamine (121-44-8) → (2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine (53662-51-4)

Guidance literature:

Reference yield: 95.0%

(2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine (53662-51-4) → 1-isothiocyanato-2-methoxybenzene (3288-04-8)

Guidance literature:

With p-toluenesulfonyl chloride; In tetrahydrofuran; at 0 - 22 ℃; for 1h;

DOI:10.1021/jo070246n

Reference yield: 46.0%

(2-methoxy-phenyl)-dithiocarbamic acid ; compound with triethylamine (53662-51-4) → 5-[(Z)-4-Chloro-phenylimino]-4-(2-methoxy-phenyl)-[1,2,4]dithiazolidine-3-thione (130256-10-9) + 4-(2-Methoxy-phenyl)-5-[(Z)-2-methoxy-phenylimino]-[1,2,4]dithiazolidine-3-thione (135472-04-7)

Guidance literature:

With N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride; In benzene; Ambient temperature;

upstream raw materials:

2-methoxy-phenylamine

triethylamine

Downstream raw materials:

5-[(Z)-4-Chloro-phenylimino]-4-(2-methoxy-phenyl)-[1,2,4]dithiazolidine-3-thione

4-(2-Methoxy-phenyl)-5-[(Z)-2-methoxy-phenylimino]-[1,2,4]dithiazolidine-3-thione

3-(2-methoxy-phenyl)-2-thioxo-2,3-dihydro-1H-quinazolin-4-one

1-isothiocyanato-2-methoxybenzene