o-xylylenebisurea

Base Information

• Chemical Name: o-xylylenebisurea
• CAS No.: 35180-29-1
• Molecular Formula: C₁₀H₁₄N₄O₂
• Molecular Weight: 222.247
• Mol file: 35180-29-1.mol

Synonyms:o-xylylenebisurea

Chemical Property of o-xylylenebisurea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-xylylenebisurea

There total 6 articles about o-xylylenebisurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

potassium cyanide (151-50-8) + α,α-diamino-o-xylene dihydrochloride (21294-14-4,92503-43-0) → o-xylylenebisurea (35180-29-1)

Guidance literature:

In water; at 20 ℃;

DOI:10.1021/jo800699s

Reference yield:

o-xylene (95-47-6) → o-xylylenebisurea (35180-29-1)

Guidance literature:

Multi-step reaction with 3 steps

1: bromine

2: hydrogenchloride; sodium azide; triphenylphosphine

3: water

With hydrogenchloride; sodium azide; bromine; triphenylphosphine; In water;

DOI:10.1007/s10870-016-0646-y

Reference yield:

α,α'-dibromo-o-xylene (91-13-4) → o-xylylenebisurea (35180-29-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; sodium azide; triphenylphosphine

2: water

With hydrogenchloride; sodium azide; triphenylphosphine; In water;

DOI:10.1007/s10870-016-0646-y

upstream raw materials:

o-Xylylene dichloride

urea

o-xylene

potassium cyanide

Downstream raw materials:

1,2-benzenedimethanamine

Refernces

• 1、 Stancl, Marek,Necas, Marek,Taraba, Jan,Sindelar, Vladimir. "Glycoluril dimers bearing hydrogen atoms on their convex face and their self-assembly in the solid state". . p. 4671 - 4675. Retrieved 2008.