Technology Process of C26H24N2O3
There total 5 articles about C26H24N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H14BrNO2; 2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)ethanol;
With
caesium carbonate;
In
1,4-dioxane; ethanol; water;
at 20 ℃;
for 0.5h;
Inert atmosphere;
Reflux;
With
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; ethanol; water;
for 12h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / N,N-dimethyl-formamide; toluene / 1 h / Inert atmosphere; Reflux
1.2: 0.5 h / 0 °C / Inert atmosphere
2.1: silver benzoate; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3.1: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 16 h / Inert atmosphere; Reflux
4.1: caesium carbonate / ethanol; water; 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere; Reflux
4.2: 12 h / Reflux
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; silver benzoate; sodium carbonate; caesium carbonate; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: silver benzoate; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
2.1: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 16 h / Inert atmosphere; Reflux
3.1: caesium carbonate / ethanol; water; 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere; Reflux
3.2: 12 h / Reflux
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; silver benzoate; sodium carbonate; caesium carbonate; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;