4-Diethylaminophenol

Base Information

• Chemical Name: 4-Diethylaminophenol
• CAS No.: 17609-82-4
• Molecular Formula: C10H15NO
• Molecular Weight: 165.235
• Hs Code.: 2922299090
• European Community (EC) Number: 241-584-9
• DSSTox Substance ID: DTXSID90170084
• Nikkaji Number: J141.510G
• Wikidata: Q83039941
• Mol file: 17609-82-4.mol

Synonyms:4-Diethylaminophenol;4-(diethylamino)phenol;17609-82-4;EINECS 241-584-9;p-diethylaminophenol;SCHEMBL387884;DTXSID90170084;ADAL1007065;STL301781;AKOS022107221;EN300-1615080

Chemical Property of 4-Diethylaminophenol

Chemical Property:

• Vapor Pressure: 0.00122mmHg at 25°C
• Boiling Point: 290°Cat760mmHg
• Flash Point: 141.5°C
• PSA: 23.47000
• Density: 1.04g/cm³
• LogP: 2.23840
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 165.115364102
• Heavy Atom Count: 12
• Complexity: 115

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC=C(C=C1)O

Technology Process of 4-Diethylaminophenol

There total 5 articles about 4-Diethylaminophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.3%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + ethanol (64-17-5) → N,N-diethyl-para-aminophenole (17609-82-4)

Guidance literature:

With Ni nanoparticles supported on N-doped mesoporous carbon pyrolyzed at 650 °C; at 240 ℃; for 4h; under 7500.75 Torr; Inert atmosphere; Green chemistry;

DOI:10.1002/cctc.202100925

Reference yield: 11.0%

N,N-diethylaniline (91-66-7) → N,N-diethyl-para-aminophenole (17609-82-4) + N,N-diethylaminophenol (35478-71-8) + 3-diethylaminophenol (91-68-9)

Guidance literature:

With dihydrogen peroxide; antimony pentafluoride; In hydrogen fluoride; at -20 ℃; for 0.25h; Mechanism; Product distribution;

Reference yield:

1-ethoxy-4-nitrobenzene (100-29-8) → N,N-diethyl-para-aminophenole (17609-82-4)

Guidance literature:

upstream raw materials:

1-ethoxy-4-nitrobenzene

N,N-diethylaniline

chloroamine-T

brilliant green

Downstream raw materials:

2-(5-Chloro-2-pyridylazo)-5-(diethylamino)-phenol

C₁₅H₂₄BrNO

C₁₅H₁₄F₄N₂O

4-((10-(diethylamino)-6,7-dioxo-6,7-dihydrochromeno[3,4-c]chromen-3-yl)oxy)-2,3,5,6-tetrafluorobenzaldehyde

Refernces

• 1、 Tao, Yuewen,Nie, Yunqing,Hu, Haitao,Wang, Ke,Chen, Yi,Nie, Renfeng,Wang, Jianshe,Lu, Tianliang,Zhang, Yongsheng,Xu, Chunbao Charles. "Highly Active Ni Nanoparticles on N-doped Mesoporous Carbon with Tunable Selectivity for the One-Pot Transfer Hydroalkylation of Nitroarenes with EtOH in the Absence of H2". . p. 4243 - 4250. Retrieved 2021/08/20.
• 2、 Jacquesy, Jean-Claude,Jouannetaud, Marie-Paule,Morellet, Guy,Vidal, Yves. "DIRECT CONVERSION OF ANILINES INTO AMINOPHENOLS". . p. 1479 - 1482. Retrieved 2007/10/02.