DIMETHALLYL ETHER

Base Information

• Chemical Name: DIMETHALLYL ETHER
• CAS No.: 628-56-8
• Molecular Formula: C8H14 O
• Molecular Weight: 126.199
• Mol file: 628-56-8.mol

Synonyms:1-Propene,3,3'-oxybis[2-methyl- (9CI); Ether, bis(2-methylallyl) (6CI,7CI,8CI);Bis(2-methyl-2-propen-1-yl) ether; Bis(2-methyl-2-propenyl) ether;Bis(2-methylallyl) ether; Bismethallyl ether; Dimethallyl ether

Chemical Property of DIMETHALLYL ETHER

Chemical Property:

• Vapor Pressure: 5.73mmHg at 25°C
• Boiling Point: 146.9°C at 760 mmHg
• Flash Point: 28.7°C
• PSA: 9.23000
• Density: 0.805g/cm³
• LogP: 2.15520

Purity/Quality:

99% ^*data from raw suppliers

DIMETHALLYL ETHER 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIMETHALLYL ETHER

There total 3 articles about DIMETHALLYL ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-hydroxy-2-methyl-1-propene (513-42-8) → isopropenylmethyl ether (628-56-8)

Guidance literature:

tetrakis(triphenyl phosphite)palladium⁽⁰⁾; at 100 ℃; for 10h;

DOI:10.1021/jo030370g

Reference yield:

3-Chloro-2-methylpropene (563-47-3) + 3-hydroxy-2-methyl-1-propene (513-42-8) → isopropenylmethyl ether (628-56-8)

Guidance literature:

With sodium hydroxide;

Reference yield:

→ isopropenylmethyl ether (628-56-8)

Guidance literature:

β-Methyl-allylalkohol, CuCl, NH4Cl;

DOI:10.1246/bcsj.42.643

upstream raw materials:

3-Chloro-2-methylpropene

3-hydroxy-2-methyl-1-propene

Downstream raw materials:

2-Iodo-2-methyl-1-(2-methyl-2-propenoxy)-3-p-toluenesulphonylpropane

2-Bromo-2-methyl-1-(2-methyl-2-propenoxy)-3-p-toluenesulphonylpropane

3,4-dimethyl-2,5-dihydro-furan

isobutyraldehyde

Refernces

• 1、 Serra,Da Silva Correa,Do Vale. "The effects of the carbonyl group in the cyclization of 1-hexenyl radicals". . p. 9463 - 9488. Retrieved 2007/10/02.