Methyldichlorophosphine

Base Information Edit

Chemical Name:Methyldichlorophosphine
CAS No.:676-83-5
Molecular Formula:CH3 Cl2 P
Molecular Weight:116.915
Hs Code.:29310099
European Community (EC) Number:211-631-8
UN Number:2845
DSSTox Substance ID:DTXSID1060978
Nikkaji Number:J34.671C
Wikipedia:Methyldichlorophosphine
Wikidata:Q81989250
Mol file:676-83-5.mol

Synonyms:Methyldichlorophosphine;676-83-5;Dichloromethylphosphine;dichloro(methyl)phosphane;Methylphosphonous dichloride;Methyl phosphonous dichloride;CH3PCl2;dichloro(methyl)phosphine;Methylphosphorus dichloride;Phosphine, dichloromethyl-;PHOSPHONOUS DICHLORIDE, METHYL-;Phosphonous dichloride, P-methyl-;EINECS 211-631-8;EC 211-631-8;PMeCl2;Dichlor(methyl)phosphin;methyldichloro-phosphine;Dichloro-methylphosphine;Methyl dichlorophosphine;Methylphosphinyldichlorid;CH3Cl2P;C-H3-Cl2-P;Dichloromethylphosphine, 96%;SCHEMBL331802;DTXSID1060978;SCHEMBL11569887;GEO-00992;MFCD00013616;AKOS015913867;UN 2845;FT-0632786;Dichloromethylphosphine, technical grade, 90%;(Methylphosphonous dichloride)

Suppliers and Price of Methyldichlorophosphine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
Methyldichlorophosphine, 97%
25g
$ 866.00

Strem Chemicals
Methyldichlorophosphine, 97%
5g
$ 217.00

Sigma-Aldrich
Dichloromethylphosphine 96%
15ml
$ 921.00

American Custom Chemicals Corporation
DICHLORO METHYLPHOSPHINE 95.00%
15ML
$ 1383.69

Alfa Aesar
Methyldichlorophosphine 97+%
5g
$ 220.00

AHH
Dichloromethylphosphine 98%
100g
$ 595.00

Total 26 raw suppliers

Chemical Property of Methyldichlorophosphine Edit

Chemical Property:

Vapor Pressure:79.3mmHg at 25°C
Melting Point:81.5 °C
Refractive Index:1.4944-1.4964
Boiling Point:81-82 °C
Flash Point:48 °C
PSA：13.59000
Density:1.3
LogP:2.40570
Storage Temp.:Flammables area
Sensitive.:Air & Moisture Sensitive
Water Solubility.:Reacts with water.
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:115.9349425
Heavy Atom Count:4
Complexity:13.5
Transport DOT Label:Poison Inhalation Hazard Spontaneously Combustible

Purity/Quality:

99.9% ^*data from raw suppliers

Methyldichlorophosphine, 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s): T,F
Hazard Codes:T-F,T,F
Statements: 34-29-23/24/25-17-14-10
Safety Statements: 8-45-43-36/37/39-33-26-16-23

MSDS Files:: SDS file from LookChem

Useful:

Chemical Classes:Toxic Gases & Vapors -> Acid Halides
Canonical SMILES:CP(Cl)Cl
Uses Methyldichlorophosphine is used to prepare difunctional phosphonoamidite coupling reagents in nucleoside chemistry and "phospha-Wittig"reagents.

Technology Process of Methyldichlorophosphine

There total 20 articles about Methyldichlorophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 34557-54-5,27936-85-2
methane

: 676-83-5
methyldichlorophosphane

Guidance literature:: With phosphorus trichloride; at 350 ℃; Temperature; Reagent/catalyst; Flow reactor;

Reference yield: 92.0%

: dichloromethylphosphine aluminum trichloride complex

: 676-83-5
methyldichlorophosphane

Guidance literature:: With sodium chloride; In octane; at 125 ℃; for 6h; Solvent; Temperature;

Reference yield: 91.2%

: 74-87-3
methylene chloride

: 676-83-5
methyldichlorophosphane

Guidance literature:: With aluminum (III) chloride; aluminium; phosphorus trichloride; In dichloromethane; at 85 ℃; for 6h; under 3750.38 Torr; Temperature; Inert atmosphere;