cyclohexyl-methyl-phosphinoyl chloride

Base Information

• Chemical Name: cyclohexyl-methyl-phosphinoyl chloride
• CAS No.: 115273-69-3
• Molecular Formula: C₇H₁₄ClOP
• Molecular Weight: 180.614
• Mol file: 115273-69-3.mol

Synonyms:cyclohexyl-methyl-phosphinoyl chloride

Chemical Property of cyclohexyl-methyl-phosphinoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of cyclohexyl-methyl-phosphinoyl chloride

There total 4 articles about cyclohexyl-methyl-phosphinoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylphosphonyl difluoride (676-99-3) + cyclohexylmagnesium bromide (931-50-0) → cyclohexyl-methyl-phosphinoyl chloride (115273-69-3)

Guidance literature:

Beim Behandeln anschliessend mit SOCl₂;

DOI:10.1021/jo01363a037

Reference yield:

Methyl-cyclohexyl-phosphinsaeure-methylester (409325-44-6) → cyclohexyl-methyl-phosphinoyl chloride (115273-69-3)

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane;

DOI:10.1021/ja01020a017

Reference yield:

Chlor-diethylamino-cyclohexyl-phosphan (70530-88-0) → cyclohexyl-methyl-phosphinoyl chloride (115273-69-3)

Guidance literature:

Multi-step reaction with 2 steps

2: PCl₅ / CCl₄

With phosphorus pentachloride; In tetrachloromethane;

DOI:10.1021/ja01020a017

upstream raw materials:

methyldichlorophosphane

cyclohexane

methylphosphonyl difluoride

cyclohexylmagnesium bromide

Downstream raw materials:

Methyl-cyclohexyl-phosphinsaeure-(-)-menthylester

cyclohexyl-methyl-thiophosphinoyl chloride

cyclohexyl-methyl-phosphinoyl fluoride