Tetrahexylammonium chloride

Base Information

• Chemical Name: Tetrahexylammonium chloride
• CAS No.: 5922-92-9
• Deprecated CAS: 140175-47-9
• Molecular Formula: C24H52 N . Cl
• Molecular Weight: 390.137
• Hs Code.: 29239000
• European Community (EC) Number: 227-653-6
• DSSTox Substance ID: DTXSID00884201
• Mol file: 5922-92-9.mol

Synonyms:tetrahexylammonium;tetrahexylammonium benzoate;tetrahexylammonium bromide;tetrahexylammonium chloride;tetrahexylammonium hydroxide;tetrahexylammonium iodide;tetrahexylammonium perchlorate;tetrahexylammonium sulfate (1:1);tetrahexylammonium thicyanate

Chemical Property of Tetrahexylammonium chloride

Chemical Property:

• Appearance/Colour: white crystalline powder
• Melting Point: 111-113 °C(lit.)
• Refractive Index: 1.6000 (estimate)
• Boiling Point: 544.68°C (rough estimate)
• PSA: 0.00000
• Density: 0.8770 (rough estimate)
• LogP: 5.12840
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 20
• Exact Mass: 389.3788284
• Heavy Atom Count: 26
• Complexity: 195

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tetrahexylammonium chloride 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCC[N+](CCCCCC)(CCCCCC)CCCCCC.[Cl-]

Technology Process of Tetrahexylammonium chloride

There total 1 articles about Tetrahexylammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + C24H52N(1+)*CH4O*Cl(1-) → tetrahexylammonium chloride (5922-92-9)

Guidance literature:

In dichloromethane; at 26 ℃; Equilibrium constant; 13.2 - 14.0 M^-1;

DOI:10.3891/acta.chem.scand.51-0270

Reference yield: 75.0%

tetrahexylammonium chloride (5922-92-9) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → C32H12BF24(1-)*C24H52N(1+)

Guidance literature:

In dichloromethane; for 24h;

DOI:10.1021/ja011809u

Reference yield: 61.0%

tetrahexylammonium chloride (5922-92-9) + benzyl-(3-methyl-2-pyridinyl)amine (70720-38-6) → 3-methyl-N-(1-phenylheptyl)pyridin-2-amine

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide; In toluene; at 140 ℃; for 16h; Inert atmosphere; Glovebox;

DOI:10.1021/acs.orglett.7b01946

upstream raw materials:

methanol

Downstream raw materials:

1-hexene

tri-n-hexylamine

tetrahexylammonium hydroxide

(S)-N-(3,5-dinitrobenzoyl)leucine

Refernces