C₂₇H₂₆Si

Base Information

• Chemical Name: C₂₇H₂₆Si
• CAS No.: 1355956-43-2
• Molecular Formula: C₂₇H₂₆Si
• Molecular Weight: 378.589
• Mol file: 1355956-43-2.mol

Synonyms:C₂₇H₂₆Si

Chemical Property of C₂₇H₂₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₆Si

There total 3 articles about C₂₇H₂₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-(phenyl)-1-(m-tolyl)ethylene (4333-70-4) + diphenylsilane (775-12-2) → C27H26Si (1355956-43-2)

Guidance literature:

With tris(pentafluorophenyl)borate; In dichloromethane; at 20 ℃;

DOI:10.1021/ol203428c

Reference yield:

1-bromovinylbenzene (98-81-7) → C27H26Si (1355956-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

2: tris(pentafluorophenyl)borate / dichloromethane / 20 °C

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tris(pentafluorophenyl)borate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol203428c

Reference yield:

m-tolylboronic acid (17933-03-8) → C27H26Si (1355956-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

2: tris(pentafluorophenyl)borate / dichloromethane / 20 °C

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tris(pentafluorophenyl)borate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol203428c

upstream raw materials:

1-bromovinylbenzene

1-(phenyl)-1-(m-tolyl)ethylene

diphenylsilane

m-tolylboronic acid

Downstream raw materials:

C₂₇H₂₄Si

Refernces