3-Chloropropylammonium chloride

Base Information

• Chemical Name: 3-Chloropropylammonium chloride
• CAS No.: 6276-54-6
• Molecular Formula: C3H9Cl2N
• Molecular Weight: 130.017
• Hs Code.: H2CH2CH2CH2·HCl MOL WT. 130.02
• Mol file: 6276-54-6.mol

Synonyms:3-Chloropropylammonium chloride

Chemical Property of 3-Chloropropylammonium chloride

Chemical Property:

• Appearance/Colour: off-white to yellow-beige crystalline
• Vapor Pressure: 9.58mmHg at 25°C
• Melting Point: 145-150 °C(lit.)
• Boiling Point: 130.7 °C at 760 mmHg
• Flash Point: 32.9 °C
• PSA: 26.02000
• Density: 1.004 g/cm3
• LogP: 2.07630
• Storage Temp.: Store below +30°C.
• Solubility.: DMSO (Slightly), Methanol (Slightly)
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 129.0112047
• Heavy Atom Count: 6
• Complexity: 16.4

Purity/Quality:

99% ^*data from raw suppliers

3-Chloropropylamine hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37-36-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C[NH3+])CCl.[Cl-]
• Uses: 3-Chloropropylamine hydrochloride was used in chemical treatment of carbon-enriched fly ash concentrates.It was used in the synthesis of linear, star and comb-like polyacrylamides by atomic transfer radical polymerization. It was used in the synthesis of halogen-functionalized aliphatic polyketones (macroinitiators). 3-Chloropropylamine hydrochloride was used in chemical treatment of carbon-enriched fly ash concentrates. It was used in the synthesis of linear, star and comb-like polyacrylamides by atomic transfer radical polymerization. It was used in the synthesis of halogen-functionalized aliphatic polyketones (macroinitiators).

Technology Process of 3-Chloropropylammonium chloride

There total 2 articles about 3-Chloropropylammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

propan-1-ol-3-amine (156-87-6) → 3-chloropropylamine hydrochloride (6276-54-6)

Guidance literature:

With thionyl chloride; In chloroform; at 0 ℃; Reflux;

Reference yield: 83.0%

3-hydroxypropylamine hydrochloride (14302-46-6) → 3-chloropropylamine hydrochloride (6276-54-6)

Guidance literature:

With thionyl chloride; at 25 ℃; for 1h;

DOI:10.1016/S0040-4020(98)01014-X

Reference yield: 100.0%

3-chloropropylamine hydrochloride (6276-54-6) → 3-azidopropylamine (88192-19-2)

Guidance literature:

With sodium azide; In water; at 80 ℃; for 15h;

DOI:10.3390/molecules22050802

upstream raw materials:

3-hydroxypropylamine hydrochloride

propan-1-ol-3-amine

Downstream raw materials:

3-benzylmercaptopropylamine

3-Chloropropyl isothiocyanate

mercapto-3 propylamine

S-(3-aminopropyl)thiosulfuric acid

Refernces

• 1、 -. "USE OF CSE INHIBITORS FOR THE TREATMENT OF CUTANEOUS INJURIES OR CONDITIONS AND SLEEP-RELATED BREATHING DISORDERS". Paragraph 00463. . Retrieved 2014/02/16.
• 2、 Geneste, Herve,Hesse, Manfred. "Synthesis of 13C-dilabeled 4-coumaroylspermidines". . p. 15199 - 15214. Retrieved 2007/10/03.