butyl 2-(4-methylbenzoyl)benzoate

Base Information

• Chemical Name: butyl 2-(4-methylbenzoyl)benzoate
• CAS No.: 51476-13-2
• Molecular Formula: C₁₉H₂₀O₃
• Molecular Weight: 296.366
• Mol file: 51476-13-2.mol

Synonyms:butyl 2-(4-methylbenzoyl)benzoate

Chemical Property of butyl 2-(4-methylbenzoyl)benzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of butyl 2-(4-methylbenzoyl)benzoate

There total 3 articles about butyl 2-(4-methylbenzoyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-methyl-benzaldehyde (104-87-0) + n-butyl 2-iodobenzoate (67330-35-2) → butyl 2-(4-methylbenzoyl)benzoate (51476-13-2)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; silver(l) oxide; In water; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.6b01064

Reference yield:

2-(4-toluoyl)benzoic acid (85-55-2) + butan-1-ol (71-36-3) → butyl 2-(4-methylbenzoyl)benzoate (51476-13-2)

Guidance literature:

With sulfuric acid;

Reference yield:

→ butyl 2-(4-methylbenzoyl)benzoate (51476-13-2)

Guidance literature:

entspr. 4'-substit. 2-Carboxy-benzophenon, wfr. HCl-Gas, Butanol-(1);

upstream raw materials:

2-(4-toluoyl)benzoic acid

butan-1-ol

4-methyl-benzaldehyde

n-butyl 2-iodobenzoate

Refernces