Technology Process of butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate
There total 1 articles about butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methyl 3-oxohept-6-enoate; N-(tert-butoxycarbonyl)-1,4-phenylenediamine; butan-1-ol;
With
sulfuric acid;
for 6h;
Heating / reflux;
4-dodecylbenzenesulphonyl azide;
With
triethylamine;
In
acetonitrile;
at 20 ℃;
for 6h;
Heating / reflux;
With
sodium nitrite;
In
water; acetonitrile;
at 20 ℃;
- Guidance literature:
-
butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate;
With
sodium hydroxide; water;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 4h;
With
hydrogenchloride;
In
tetrahydrofuran; methanol; water;