[Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n

Base Information

• Chemical Name: [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n
• CAS No.: 1311149-22-0
• Molecular Formula: C₈H₄O₅*C₁₂H₉N₃*Cd
• Molecular Weight: 487.75
• Mol file: 1311149-22-0.mol

Synonyms:[Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n

Chemical Property of [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n

Chemical Property:

Purity/Quality:

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Technology Process of [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n

There total 2 articles about [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]_n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-(2'-pyridyl)benzimidazole (1137-68-4) + cadmium(II) sulfate hexahydrate + 5-Hydroxyisophthalic acid (618-83-7) → [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]n (1311149-22-0)

Guidance literature:

With Et₃N; In methanol; water; High Pressure; metal compd. (1 mmol) added to soln. of 2-PBIM (1 mmol) and acid (1 mmol) in MeOH/H2O (1/3, v/v), pH 8.0 (Et3N), sealed, heated at 160°C for 72 h; cooled, filtered off, washed (H2O), dried in air, elem. anal.;

DOI:10.1016/j.ica.2011.02.092

Reference yield: 19.0%

2-(2'-pyridyl)benzimidazole (1137-68-4) + cadmium(II) nitrate tetrhydrate + 5-Hydroxyisophthalic acid (618-83-7) → [Cd(5-hydroxyisophthalic acid)(2-(2-pyridyl)benzimidazole)]n (1311149-22-0)

Guidance literature:

With triethylamine; In water; acetonitrile; at 140 ℃; for 120h; Autoclave;

DOI:10.1080/10610278.2014.959015

upstream raw materials:

2-(2'-pyridyl)benzimidazole

5-Hydroxyisophthalic acid

Refernces

• 1、 Li, Jing,Ji, Chang-Chun,Huang, Liang-Fang,Li, Yi-Zhi,Zheng, He-Gen. "Syntheses, structures, luminescent and magnetic properties of a novel class of metal complexes constructed from 2-(2-pyridyl)benzimidazole and 5-hydroxy-1,3-benzenedicarboxylic acid". . p. 27 - 35. Retrieved 2011/06/21.