8-bromo-1-octanal

Base Information

• Chemical Name: 8-bromo-1-octanal
• CAS No.: 92540-33-5
• Molecular Formula: C₈H₁₅BrO
• Molecular Weight: 207.111
• Mol file: 92540-33-5.mol

Synonyms:8-bromo-1-octanal

Chemical Property of 8-bromo-1-octanal

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 8-bromo-1-octanal

There total 1 articles about 8-bromo-1-octanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclooctanol (696-71-9) → 9-oxa-bicyclo[4.2.1]nonane (284-20-8) + cycloactanone (502-49-8) + 8-bromo-1-octanal (92540-33-5)

Guidance literature:

With lead(IV) acetate; potassium bromide; In benzene; at 80 ℃; Yield given. Yields of byproduct given;

DOI:10.1007/BF00959880

Reference yield: 65.0%

1-methoxy-4-(3,3,3-trifluoroprop-1-en-2-yl)benzene (69843-08-9) + 8-bromo-1-octanal (92540-33-5) → 11-bromo-1,1-difluoro-2-(4-methoxyphenyl)undec-1-en-4-ol

Guidance literature:

1-methoxy-4-(3,3,3-trifluoroprop-1-en-2-yl)benzene; 8-bromo-1-octanal; With chromium chloride; chloro-trimethyl-silane; 4,4'-di-tert-butyl-2,2'-bipyridine; zinc; In N,N-dimethyl acetamide; at 40 ℃; for 16h; Schlenk technique; Inert atmosphere;

With hydrogenchloride; In N,N-dimethyl acetamide; water; for 1h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.1c04531

Reference yield: 53.0%

1'-acetoxyestragole (61691-82-5) + 8-bromo-1-octanal (92540-33-5) → (E)-11-bromo-1-(4-methoxyphenyl)undec-1-en-4-one

Guidance literature:

With nickel(II) bromide dimethoxyethane; 4,7-Dimethyl-1,10-phenanthroline; tetrakis(tetrabutylammonium)decatungstate(VI); In acetonitrile; at 45 ℃; for 12h; stereoselective reaction; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.1c02938

upstream raw materials:

cyclooctanol

Downstream raw materials:

9-bromo-1-nonene

(Z)-(R)-14-methylhexadec-8-ene-1-al dimethyl acetal

(R)-(-)-benzyl N-(9-bromo-2-hydroxynonyl)carbamate

2-(benzenesulfonyl)-9-{3-[1-(((tert-butyldimethylsilanyl)oxy)methyl)vinyl]oxiran-2-yl}nonanoic acid methyl ester

Refernces