3-phenyl-2-nitronapthalene

Base Information

• Chemical Name: 3-phenyl-2-nitronapthalene
• CAS No.: 92795-23-8
• Molecular Formula: C₁₆H₁₁NO₂
• Molecular Weight: 249.269
• Mol file: 92795-23-8.mol

Synonyms:3-phenyl-2-nitronapthalene

Chemical Property of 3-phenyl-2-nitronapthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenyl-2-nitronapthalene

There total 5 articles about 3-phenyl-2-nitronapthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C16H13NO2 (1450995-35-3) → 3-phenyl-2-nitronapthalene (92795-23-8)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In 1,2-dichloro-ethane; for 10h; Reflux; Inert atmosphere;

DOI:10.1055/s-0033-1338867

Reference yield: 86.0%

→ 3-phenyl-2-nitronapthalene (92795-23-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃;

Reference yield: 69.0%

2-bromo-3-nitronaphthalene (67116-33-0) + phenylboronic acid (98-80-6) → 3-phenyl-2-nitronapthalene (92795-23-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; toluene; for 12h; Reflux;

upstream raw materials:

benzene

3-nitronaphthalen-2-amine

C₁₆H₁₃NO₂

2-bromo-3-nitronaphthalene

Downstream raw materials:

2-amino-3-phenyl-naphthalene

3‐phenylnaphthalen‐2‐ol

(+/-)-3,3'-diphenyl-1,1'-binaphthyl-2,2'-diamine

2,3-benzocarbazole

Refernces

• 1、 -. "COMPOUND FOR ORGANIC ELECTRONIC ELEMENT, ORGANIC ELECTRONIC ELEMENT USING THE SAME, AND AN ELECTRONIC DEVICE THEREOF". Paragraph 0124; 0154; 0155; 0160; 0161. . Retrieved 2016/10/08.