alpha-Chlorobenzaldehyde O-mesyl oxime

Base Information Edit

Chemical Name:alpha-Chlorobenzaldehyde O-mesyl oxime
CAS No.:5023-82-5
Molecular Formula:C8H8 Cl N O3 S
Molecular Weight:233.675
Hs Code.:
NSC Number:529360
DSSTox Substance ID:DTXSID20423015
Nikkaji Number:J2.691.762J
Mol file:5023-82-5.mol

Synonyms:NSC529360;5023-82-5;SCHEMBL15389722;DTXSID20423015;alpha-Chlorobenzaldehyde O-mesyl oxime;NSC-529360

Suppliers and Price of alpha-Chlorobenzaldehyde O-mesyl oxime

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of alpha-Chlorobenzaldehyde O-mesyl oxime Edit

Chemical Property:

Vapor Pressure:0.000227mmHg at 25°C
Boiling Point:335.8°Cat760mmHg
Flash Point:156.9°C
Density:1.35g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:232.9913420
Heavy Atom Count:14
Complexity:301

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)ON=C(C1=CC=CC=C1)Cl
Isomeric SMILES:CS(=O)(=O)O/N=C(\C1=CC=CC=C1)/Cl

Technology Process of alpha-Chlorobenzaldehyde O-mesyl oxime

There total 4 articles about alpha-Chlorobenzaldehyde O-mesyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 698-16-8
benzohydroximoyl chloride

: 5023-82-5
N-((methylsulfonyl)oxy)benzimidoyl chloride

Guidance literature:: With triethylamine;
DOI:10.1139/v66-041

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 932-90-1
Benzaldoxime

: 5023-82-5
N-((methylsulfonyl)oxy)benzimidoyl chloride

Guidance literature:: Benzaldoxime; With N-chloro-succinimide; In tetrahydrofuran; chloroform; at 40 ℃; for 1h;

With triethylamine; In ethyl acetate; at 0 ℃; for 0.166667h;

methanesulfonyl chloride; In ethyl acetate; at 0 - 20 ℃; for 1h;
DOI:10.1039/c5ra10060g

Reference yield:

: 5023-82-5
(E)-N-((methylsulfonyl)oxy)benzimidoyl chloride

Guidance literature:: With hydrogenchloride; N-chloro-succinimide; In 2-methyltetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; at 10 - 20 ℃; for 0.5h;

With N-ethyl-N,N-diisopropylamine; In 2-methyltetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; at 10 - 20 ℃; for 1h;