ethoxy-dichloro-acetyl chloride

Base Information

• Chemical Name: ethoxy-dichloro-acetyl chloride
• CAS No.: 98019-44-4
• Molecular Formula: C₄H₅Cl₃O₂
• Molecular Weight: 191.441
• Mol file: 98019-44-4.mol

Synonyms:ethoxy-dichloro-acetyl chloride

Chemical Property of ethoxy-dichloro-acetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethoxy-dichloro-acetyl chloride

There total 4 articles about ethoxy-dichloro-acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

oxalic acid diethyl ester (95-92-1) → oxalyl dichloride (79-37-8) + chloroethane (75-00-3) + 1,2-diethoxy-tetrachloro-ethane (63938-37-4) + ethoxy-dichloro-acetyl chloride (98019-44-4) + Ethyl oxalyl chloride (4755-77-5)

Guidance literature:

With phosphorus pentachloride; manganese(ll) chloride; at 90 ℃; for 5h; Product distribution; other catalysts (CuCl₂, ZnCl₂, CdCl₂, CrCl₃, FeCl₃, CoCl₂, PdCl₂) and temperatures (from 70 to 130 deg C);

Reference yield:

1,2-diethoxy-tetrachloro-ethane (63938-37-4) → oxalyl dichloride (79-37-8) + chloroethane (75-00-3) + ethoxy-dichloro-acetyl chloride (98019-44-4)

Guidance literature:

at 165 ℃;

Reference yield:

1,2-diethoxy-1,2-dichloro-ethane (57987-56-1) + iodine (7553-56-2,12190-71-5,8031-47-8) + chlorine (7782-50-5) → chloroethane (75-00-3) + ethoxy-dichloro-acetyl chloride (98019-44-4)

Guidance literature:

at 150 ℃;

upstream raw materials:

1,2-diethoxy-tetrachloro-ethane

oxalic acid diethyl ester

1,2-diethoxy-1,2-dichloro-ethane

iodine

Refernces